ISSN 0030-400X, Optics and Spectroscopy, 2014, Vol. 116, No. 6, pp. 897–905. © Pleiades Publishing, Ltd., 2014.
Original Russian Text © I.V. Romanova, B.Z. Malkin, M.S. Tagirov, 2014, published in Optika i Spektroskopiya, 2014, Vol. 116, No. 6, pp. 973–981.
897
INTRODUCTION
Over the last three decades, double lithium–rare-
earth fluorides LiLnF
4
(Ln denotes the rare-earth ion)
have been studied intensely due to a variety of their
magnetic properties [1–5]. Simulation of magnetic-
field effects in LiLnF
4
single crystals is an important
problem for the development of the theory of magne-
toelastic effects in magnetically concentrated crystals
that contain rare-earth ions.
LiLnF
4
crystals have a tetragonal structure of
scheelite CaWO
4
; their space-symmetry group is
(I4
1
/a); the unit cell contains two magnetically equiv-
alent Ln
3+
ions at sites with the S
4
point-symmetry
group [6]. LiTmF
4
is a dielectric van Vleck paramagnet
[7], a distinctive feature of which is a strong magne-
toelastic interaction, which is evidenced by a giant
magnetostriction, which was revealed in [8], and char-
acteristic extrema in temperature dependences of elas-
tic constants [9, 10]. The authors of [11, 12], using
optical-spectroscopy methods, have observed a sub-
stantially nonlinear and anisotropic dependence of the
splitting of the first excited doublet of Tm
3+
ions on the
external magnetic field that was oriented in the base
plane of the LiTmF
4
crystal, which is caused by the
magnetoelastic interaction. Later, the authors of [13,
14] measured the dependences of the magnetization of
LiTmF
4
single crystals on the magnitude and direction
of the magnetic field at different temperatures. Results
of calculations of piezospectroscopic effects [15],
magnetostriction [8, 10], and nonlinear Zeeman
effect [11, 12], which were done in terms of the model
of a linear electron–deformation interaction, agree
well with measurement data; however, the values of
coupling parameters of thulium ions with lattice
deformations that were used in these works differ con-
C
4 h
6
siderably from the values of corresponding parameters
that were found from the analysis of the data of
piezospectroscopic investigations of thulium and hol-
mium impurity ions in an isostructural crystal LiYF
4
[16, 17]. It should be noted that the previous analysis
of the experimental data was performed taking into
account only the magnetic-dipole–dipole interaction
between rare-earth ions, which, in the case of the van
Vleck paramagnet, plays an insignificant role at low
temperatures. The revealed strong interaction of Tm
3+
ions with static lattice deformations is indicative of the
possibility of an efficient multipole interaction
between thulium ions that is caused by exchange of
phonons. The multipole interaction leads to the
renormalization of parameters of an effective one-par-
ticle Hamiltonian and, as was noted in [15], can be the
reason for the difference between parameters of the
electron–phonon interaction in magnetically concen-
trated and diluted systems. The objective of this work
is to calculate the parameters of the Hamiltonian of
the interaction between thulium ions using previously
found characteristics of the electron–phonon interac-
tion and the lattice dynamics of LiLnF
4
crystals [18–
20] and to construct a self-consistent model for the
calculation of magnetic and magnetoelastic charac-
teristics of the LiTmF
4
crystal taking into account
multipole interactions.
THEORETICAL SUBSTANTIATION
OF THE MODEL
The Hamiltonian of the magnetic subsystem,
which consists of thulium ions interacting with the
crystal lattice with a free surface, will be written as
XV INTERNATIONAL
FEOFILOV SYMPOSIUM
Multipole Interactions in a LiTmF
4
Single Crystal
I. V. Romanova, B. Z. Malkin, and M. S. Tagirov
Kazan (Volga Region) Federal University, Kazan, 420008 Tatarstan, Russia
e-mail: Irina.Choustova@kpfu.ru
Received November 18, 2013
Abstract—We have considered magnetic and magnetoelastic characteristics of a van Vleck paramagnet
LiTmF
4
taking into account the interaction between thulium ions via the phonon field. We have calculated
parameters of the multipole interaction that is caused by the interaction of Tm
3+
ions with dynamic lattice
deformations of the B
g
symmetry. We have presented a self-consistent description of previously published
results of measurements of temperature dependences of elastic constants and the nonlinear Zeeman effect in
the optical spectrum of the LiTmF
4
single crystal, as well as dependences of the magnetostriction on temper-
ature, magnitude, and direction of the external magnetic field.
DOI: 10.1134/S0030400X14060198