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BMC Biotechnology
Open Access
Methodology article
Simple and efficient site-directed mutagenesis using two
single-primer reactions in parallel to generate mutants for protein
structure-function studies
Oded Edelheit
1,2,3
, Aaron Hanukoglu
2,3
and Israel Hanukoglu*
1
Address:
1
Department of Molecular Biology, Ariel University Center, Ariel, Israel,
2
Department of Pediatrics, Tel-Aviv University, Sackler Medical
School, Tel Aviv, Israel and
3
Division of Pediatric Endocrinology, E. Wolfson Medical Center, Holon, Israel
Email: Oded Edelheit - ede.oded@gmail.com; Aaron Hanukoglu - aaronh@science.co.il; Israel Hanukoglu* - mbiochem@gmail.com
* Corresponding author
Abstract
Background: In protein engineering, site-directed mutagenesis methods are used to generate
DNA sequences with mutated codons, insertions or deletions. In a widely used method, mutations
are generated by PCR using a pair of oligonucleotide primers designed with mismatching
nucleotides at the center of the primers. In this method, primer-primer annealing may prevent
cloning of mutant cDNAs. To circumvent this problem we developed an alternative procedure that
does not use forward-reverse primer pair in the same reaction.
Results: In initial studies we used a double-primer PCR mutagenesis protocol, but sequencing of
products showed tandem repeats of primer in cloned DNA. We developed an alternative method
that starts with two Single-Primer Reactions IN Parallel using high-fidelity Pwo DNA polymerase.
Thus, we call the method with the acronym SPRINP. The SPRINP reactions are then combined,
denatured at 95°C, and slowly cooled, promoting random annealing of the parental DNA and the
newly synthesized strands. The products are digested with DpnI that digests methylated parental
strands, and then transformed into E. coli. Using this method we generated >40 mutants in cDNAs
coding for human Epithelial Na
+
Channel (ENaC) subunits. The method has been tested for 1–3 bp
codon mutation and insertion of a 27 bp epitope tag into cDNAs.
Conclusion: The SPRINP mutagenesis protocol yields mutants reliably and with high fidelity. The
use of a single primer in each amplification reaction increases the probability of success of primers
relative to previous methods employing a forward and reverse primer pair in the same reaction.
Background
Site-directed mutagenesis (SDM) methods are used to
generate cloned DNAs with modified sequences for exam-
ining the importance of specific residues in protein struc-
ture and function. SDM represents the primary rational
method in protein engineering and for altering enzyme
substrate selectivity [1,2].
Currently prevalent methods of SDM employ PCR using
oligonucleotide primer pairs that carry the desired muta-
tion. There is a large variety of approaches for SDM using
PCR [1,3,4]. One of the widely used methods is Quik-
Change [5]. This method and its later modifications
employ complementary primer pairs in the same PCR
reaction. The use of complementary primer pairs may lead
Published: 30 June 2009
BMC Biotechnology 2009, 9:61 doi:10.1186/1472-6750-9-61
Received: 26 February 2009
Accepted: 30 June 2009
This article is available from: http://www.biomedcentral.com/1472-6750/9/61
© 2009 Edelheit et al; licensee BioMed Central Ltd.
This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/2.0 ),
which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.