Low Temperature Microwave Characterisation of GreenTapes using
Split Post Dielectric Resonator
M. V. Jacob
1
, S. Thomas
2
, M. Sebastian
2
, J. Mazierska
3, 1
,
J. Honkama
4
and H. Jantunen
4
,
1
Electronic Material Research Laboratory, School of Engineering,
James Cook University, Townsville QLD 4811 Australia
2
National Institute for Interdisciplinary Science and Technology
Trivandrum 695019, India
3
Massey University, School of Engineering and Advanced Technology, New Zealand
4
INFOTECH, University of Oulu, Finland
1
mohan.jacob@jcu.edu.au
Abstract – Investigation into the fabrication of dielectric materials suitable for low
temperature co-fired ceramic (LTCC) applications and their characterisation at high
frequencies is a prominent research area. There has been number of papers featuring the
analyses of performance of LTCC materials at microwave frequencies published. However
there are no reports presenting microwave properties of source materials, before firing takes
place, (Greentape). High frequency dielectric properties of Greentape material in the
temperature range from 10K to 290 K using a split post dielectric resonator has been
presented in this paper. We investigated two Greentape materials of differing thicknesses
(0.08 mm and 0.13 mm) at a frequency of 10 GHz.
INTRODUCTION
Low Temperature Co-fired ceramic (LTCC) is one of the most powerful Multi Chip Module
(MCM) technologies for wireless communication circuits. The main advantage of the LTCC
is the fabrication of three-dimensional circuits, in which resistors, inductors, capacitors and
low loss interconnects are “buried” within a ceramic block, resulting in high integration,
hermetical sealing and electromagnetic shielding. Due to the advantages of this technology
the LTCC-based components are used in commercial microwave applications such as WLAN
transceivers, cellular telephony and portable wireless devices [1-6].
Further advancement can be achieved by identifying new materials suitable for the LTCC
technology and improving the existing ones [4-6]. Since the materials are likely to find
applications at higher frequencies and varying ambient environment, it is important to
investigate their microwave properties at differing temperatures.
For fabrication of Low Temperature Co-fired Ceramics, thin layers of materials referred to as
‘Greentape’ are used despite the colour before firing being usually white, not green. The
thickness of LTCC materials is controlled by adding more layers of Greentape, and this
process could change the microwave losses of the resulting LTCC structure. This paper aims
to precisely measure the microwave properties of a greentape material of low ε
r
of two
differing thickness as a function of temperature.
EXPERIMENTS
Powder preparation
The 0.83 ZnAl
2
O
4
-0.17 TiO
2
(ZAT) ceramics were prepared by the conventional solid state
ceramic route [7]. High purity ZnO [Aldrich Chemical Company, 99.9%] and Al
2
O
3
[Alcoa
A16SG] were used as starting materials for the synthesis of ZnAl
2
O
4
. The chemicals were
stoichiometrically weighed and were ball milled in polyethylene bottle using Zr balls in
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