International Journal of Engineering and Technology Volume 4 No. 5, May, 2014
ISSN: 2049-3444 © 2014 – IJET Publications UK. All rights reserved.
325
Mechanical Properties Enhancement of Conventional Mild Steel For
Fastener Application
O. I. Sekunowo
1
, S. O. Adeosun
2
and O. E. Ojo
3
1, 2
Department of Metallurgical and Materials Engineering, University of Lagos
3
Federal Institute of Industrial Research Oshodi (FIIRO), Lagos
ABSTRACT
Due to the rampant brittle fracture of most mild steel fasteners, an innovative hardening process of microstructure modificaton is
employed on conventional mild steel to enhance its mechanical properties. The steel specimens were subjected to inter-critical
austenitising heat treatment in the temperature range of 800
0
-950
0
C and soaked for 30 minutes, quenched in water at ambient
temperature and tempered at varying temperatures of 250
0
, 350
0
, 450
0
and 550
0
C. Results of mechanical characterisation of the test
specimens demonstrate improvement in ultimate tensile strength and impact energy by 58.3 and 53.8 percent respectively coupled with
a modest increase in hardness from 25.7HRB to 37.5HRB. Contribution to improved mechanical properties stem from the inducement
of fine needle-like lower bainite particles within the dislocation-rich ferrite matrix at 450
0
C and 550
0
C tempering temperature regime.
Keywords: Mild steel, hardening, austenitising, mechanical properties
1. INTRODUCTION
Mechanical joining of engineering components is commonly
carried out using various types of materials. Besides welding
and laser processes, fastening is another veritable joining
technique depending on the service environment. Mild steel
due to its availability coupled with a relatively low cost is often
employed as metallic fasteners. However, the rampant brittle
fracture of mild steel fasteners such as nails, screws, studs, etc
on application of sudden load has become a growing concern
(Teresa and Manuela, 2008). Various reasons have been
adduced for the abysmal failure of mild steel fasteners in
service. Hence, the imperative of devising a means by which
the impact property and other relevant characteristics of
conventional mild steel can be improved. Major impact
toughness enhancement techniques that have been employed
include alloying, heat treatment and most recently, impulse
electric current treatment. Varied amounts of copper, titanium
and nickel have been added to steel by quite a number of
researchers to achieve improved impact toughness. In the work
of Mone and Scott (2011), significant improvement in impact
property was obtained as the copper content was increased
from 0.2-1.5wt%.
Enhanced impact toughness was noticed from 0.25% copper
and peaked at 1.5wt%. Philip and Richard (1970) achieved
improved toughness as the silicon content was increased.
Zirconium, titanium and nickel have also been employed by
other researchers. Although the alloying technique of
toughness enhancement has been found to be remarkably
effective, the rather prohibitive cost implication has rendered
the method unpopular except in situations where the service
benefits by far outweigh the cost burden. High impulse electric
current technique (IECT) was employed by to increase the
impact toughness of low carbon steel (Stepanov, et al., 2007).
The high-density current passed through the specimen seemed
to affect only the grain size and not the morphology. Therefore
contribution to improved toughness was reported to have been
due to the homogeneous dispersion of grains within the matrix
occasioned by the passage of impulse current. However, it has
been observed that IECT toughness enhancement has limited
applications especially in structural components.
The foregoing, properties optimisation techniques
notwithstanding the heat treatment option of impact toughness
improvement may be most versatile considering the volume of
works carried out in that area. Heat treatment involves a cycle
of heating and cooling that alters the material microstructures
resulting in a modified mechanical properties. Of the various
heat treatment methods, hardening through quenching
followed by tempering has been established as the most
effective method of enhancing the strength characteristics of
metal and their alloy. According to Offor and Ezekoye (2011),
improved notch impact toughness was exhibited by 0.14wt%
carbon steel after being subjected to varied inter-critical
(810
0
C-890
0
C) normalizing. Similarly, the hardening of HT
480 and HT 600 having 0.27wt%C (HT represents high tensile)
and subsequent quenching in oil followed by tempering
between 480
o
C and 600
o
C resulted in impact energy of 195J
and 225J respectively (Muhammed; et al., 2011). One of the
major processing parameters in hardening heat treatment is the
tempering temperature. Rugly and Strohaecker (2004) worked
on toughness improvement of low carbon steel independent of
the austenitising temperature. The result established that a
relatively high tempering temperature between 500
0
C and
650
0
C favours improved impact toughness. This was also
corroborated by Danilo and Jaime, (2010) and further
strengthened by the findings of Dosseth and Boyer, 2006 in
which it was observed that tempering in the range of 250
0
C-
370
0
C should be avoided to stem the phenomenon of temper
embritlement. Considering all of the above, the issues germane
in the heat treatment of low carbon steel for mechanical
properties enhancement bore down to the interplay of three
parameters namely the austenitising temperature, cooling rate