Desalination 148 (2002) 187–191
Presented at the International Congress on Membranes and Membrane Processes (ICOM), Toulouse, France,
July 7–12, 2002.
0011-9164/02/$– See front matter © 2002 Elsevier Science B.V. All rights reserved
*Corresponding author.
Biopolymer purification by ultrafiltration
J. Jorda, P. Marechal, L. Rigal, P.-Y. Pontalier*
Laboratoire de chimie Agro-industrielle (LCA-CATAR), 118, route de Narbonne, F31077 Toulouse cedex 4, France
Tel. +33 (5) 62885719; Fax +33 (5) 62885730; emails: jjorda@ensct.fr, pmarechal@ensct.fr, lrigal@ensct.fr,
pont@ensct.fr
Received 8 February 2002; accepted 11 March 2002
Abstract
Ultrafiltration has been investigated for the concentration of diluted biopolymer solutions. Trials were realized
with membranes of different molecular weight cut off (MWCO) and configuration modules. Results indicates that
hollow fiber module gives the best results with the membrane of 6 kilodalton (kD). Arabinoxylan solutions were
concentrated with a ratio of 2.4 and a final permeate flux of 14.5 L/h.m
2
. Rhamnogalacturonan solutions were
concentrated with a ratio of 5 and a final permeate flux of 25 L/h.m
2
.
Keywords: Ultrafiltration; Biopolymer; Concentration; Polarization; Fouling; Viscosity
1. Introduction
The technological properties (emulsifier,
thickener, gelling, film forming, coating agent)
of biopolymers make them attractive for many
industrial applications [1]. Among these polymers
arabinoxylans and rhamnogalacturonan are
polymers extracted from crops products.
Extraction stage has to disrupt cell walls, using
mechanic and chemical forces, which therefore
leads to complex solutions. Purification of such
solutions is rather difficult with many steps
combining, depending on the polymer, centri-
fugation, filtration and alcoholic precipitation [2–
3]. Precipitation is very expensive because extrac-
tion lead to very dilute solutions and precipitation
needs several volume of alcohol for one volume
of solution. Ultrafiltration could be included for
purification and concentration before spray drying
[2,4]. Ultrafiltration is a very attractive technique
for the concentration of sensitive solution because
it can be used at room temperature. The MWCO
of the membrane are usually about 10–20 kDa [5],
even some authors used 300 kDa [6] or 3 kDa
membranes [4]. Optimal conditions are not easily