IEEE TRANSACTIONS ON APPLIED SUPERCONDUCTIVITY, VOL. 20, NO. 3, JUNE 2010 1549
Electrical and Mechanical Characterization of Coated
Conductors Lap Joints
G. Celentano, A. Augieri, A. Mauretti, A. Vannozzi, A. AngrisaniArmenio, V. Galluzzi, S. Gaudio, A. Mancini,
A. Rufoloni, I. Davoli, C. Del Gaudio, and F. Nanni
Abstract—Electrical and mechanical characterizations of YBCO
coated conductors diffusion joints obtained in a 2 mm wide, Cu
stabilizer free commercial tape provided by SuperPower Inc. were
reported. Two conductor pieces were overlapped for a length of
20 mm and kept in contact under a pressure as high as 80 MPa.
A face-to-face approach was used, with or without an additional
Ag tape insert. The joint was realized by Ag diffusion at a tem-
perature of 200 and 400 C in N and O atmosphere, respectively.
The resistivity of the joint was measured at 77 K in N bath. The
mechanical properties of the joint were characterized by means of
single-lap tensile test operated at room temperature at a rate of
0.5 mm/min. The best results were obtained by high temperature
joining in O atmosphere. The resistivity of the joints was as low
as m . This value is almost halved if an Ag insert
is used. The mechanical properties of the joints are strongly de-
pendent on the use of an Ag insert, since maximum load as high
as 60 N can be applied if no additional insert is used. This value
enhances to about 100 N when an Ag insert is employed. How-
ever, the joint obtained at low temperature in N atmosphere is
also interesting since the joint resistivity was slightly increased to
m and a maximum load as high as 50 N was ob-
tained indicating that diffusion joints can be safely handled. These
results are promising in perspective of oxygen free diffusion joints
in Cu stabilized coated conductors.
Index Terms—Ag, coated conductors, diffusion joints, single-lap
test, YBCO.
I. INTRODUCTION
T
HE development of joining technology of HTS Re-123
based coated conductors is a key issue towards their prac-
tical application. In spite of the remarkable progress registered
during the last decade in the field of HTS coated conductors,
only few studies on joint processing were reported to date
[1]–[4]. Mainly, three types of joining techniques were taken
into consideration: superconducting joint, non-superconducting
joint using a low melting temperature soldering material and
diffusion joint. Anyway, the reliability of a joint technique is
strictly dependent on the application. For large scale power
Manuscript received October 19, 2009. First published April 05, 2010; current
version published May 28, 2010.
G. Celentano, A. Augieri, A. Mauretti, A. Vannozzi, A. Angrisani Armenio,
V. Galluzzi, S. Gaudio, A. Mancini, and A. Rufoloni are with ENEA-EU-
RATOM, I-00044 Frascati, Italy (e-mail: celentano@frascati.enea.it).
I. Davoli is with University Tor Vergata, 00133 Rome, Italy.
F. Nanni and C. Del Gaudio are with INSTM-Research Unit of Department
of Science and Chemical Technologies-University Tor Vergata, 00133 Rome,
Italy.
Color versions of one or more of the figures in this paper are available online
at http://ieeexplore.ieee.org.
Digital Object Identifier 10.1109/TASC.2010.2043833
applications, the last two techniques are considered the most
appropriate. On the other hand, diffusion joint, which does not
use soldering material, but just involves interdiffusion of Ag
stabilizing layers, is expected to reduce the resistance across
the joint because there is no additional resistance of a soldering
material and contact resistance. Thus, for the joining of the
superconducting tapes it is generally believed that the diffusion
joint technique is most applicable.
Previous studies have shown that with diffusion technique
joints obtained in overlapped single tapes retained high critical
current and exhibited very low contact resistivity [1], [5],
[6]. The coated conductor tape consists of a multi-layered struc-
ture composed mainly by a flexible metallic substrate (Stain-
less Steel, Hastelloy or nickel based alloys) coated by YBCO
films, the protective Ag layer, and an optional Cu stabilizer [7].
The diffusion joint technique was used only in case of Cu stabi-
lizer free and/or Cu stabilizer removed samples because of the
highly oxidizing conditions used in these studies [1], [5], [6]. By
controlling the main parameters governing the diffusion process
such as temperature, time duration and surface condition con-
tact resistivity as low as m can be reached when joints
are heated up to 500 C, demonstrating that joint resistance is
ultimately governed by the YBCO/Ag interface properties [1].
Considering that, similar joint resistivity can be achieved even
for lower joint processing temperatures provided that diffusion
between Ag layers is sufficiently promoted. For temperature in
the range of 200–300 C, the joint processing can be performed
in nitrogen atmosphere without, in principle, significant YBCO
oxygen losses and thus performance degradation [8], [9].
In this paper joint between the Ag sides of two coated con-
ductors using Ag diffusion technique are prepared and electri-
cally and mechanically characterized. For this purpose commer-
cial YBCO stabilizer free coated conductors, named SF2050,
manufactured by SuperPower Inc., have been employed. Joints
are obtained at both 200 and 400 C in nitrogen and oxygen at-
mosphere, respectively. The insertion in the joint area of an ad-
ditional thin Ag tape reduces the contact resistance. Low con-
tact resistivity, m has been achieved without any
degradation of the flowing across the joint. Mechanical test
showed high resistance to tensile load which is greatly improved
with additional Ag tape.
II. EXPERIMENTAL
This work has been carried out with stabilizer free com-
mercial YBCO coated conductors (type SF2050 manufactured
by SuperPower Inc.). The 2 mm wide tape is a IBAD-coated
conductor fabricated on 50 m thick Hastelloy C276 substrate.
Considering the sequence of the buffer layer architecture,
1051-8223/$26.00 © 2010 IEEE