Investigation and Modeling of Extraction
Parameters of Ruta chalepensis L. Essential Oil
Jamel Mejri
1
*, Manef Abderrabba
1
, Mondher Mejri
2
1
Unité de recherche en physico-chimie moléculaire, Institut Préparatoire
des Etudes Scientifiques et Techniques, IPEST, BP51, La Marsa 2070, Tunisia
2
Département de Génie des Procédés, Institut Supérieur des
Etudes Technologiques de Zaghouan, 1121 Mograne, Tunisia
Abstract: To evaluate the effects of hydrodistillation parameters and the vegetative cycle of the plant
(Ruta chalepensis L.) on the global essential oil yield the response surface methodology was used. The
parameters tested are the volume of water in the suspension to be distilled and the time of distillation. The
third parameter is the vegetative cycle of the plant. The responses were the global extraction yield and the
extraction yield of following essential oil compounds: 2-undecanone, 2-decanone, 2-dodecanone and 2-
tridecanone. The optimal conditions selected for the total output of the extraction obtained from the analysis
of the response surfaces are: time of distillation: 120 minutes; volume of water in the suspension to be distilled:
500 ml; stage of vegetation: January (young growths). The results show that the time of distillation and the
stage of vegetation are the parameters more meaning on the global essential oil yield.
Key words: Ruta chalepensis L.; Extraction; Hydrodistillation; Essential oil; Response Surface
Methology.
Introduction
An essential oil is a volatile mixture of organic
compounds derived from odorous plant material
by physical means
5
. Essential oils are very known
by their biological properties and activities in
various fields such as the agroalimentary,
pharmacy and phytotherapy. They are natural
antioxydants: they can be an alternative source
of compounds able to protect the lipids in food.
Indeed, there is an important interest for the use
of antioxydants in food industry, not only like
method of safeguarding but also for their
beneficial effects on human health
4,6,18,22
. Many
studies showed that the essential oils of some
plants can be used as inhibitors of the reactions
of oxidation of the lipids and the proteins
7
.
Essential oils are also used as antibacterial and
antifungal activities
14,21,23
.
However, these properties may change under
the action of certain parameters such as drying,
extraction method and stage of vegetation. Drying
and drying methods affect yield and essential oils
on the chemical composition. The physical
properties and antioxidant activity are also
affected by drying methods
2,13,17
.
The effects of the distillation methods and stage
of vegetation were also studied in Satureja
hortensis; the highest yield of essential oil was
Journal of Essential Oil Bearing Plants
ISSN Print: 0972-060X Online: 0976-5026
www.jeobp.com
*Corresponding author (Jamel Mejri)
E-mail: < jmejri2001@yahoo.fr > © 2012, Har Krishan Bhalla & Sons