Soft Nanoscience Letters, 2013, 3, 11-13
doi:10.4236/snl.2013.31003 Published Online January 2013 (http://www.scirp.org/journal/snl)
11
Composite Materials Containing Perfluorinated and
Siloxane Units for Vertical Alignment of Liquid Crystals
*
Rasha Ata Alla
1
, Gurumurthy Hegde
1,2
, Lachezar Komitov
1#
, Andrea Morelli
3
, Emo Chiellini
3
,
Giancarlo Galli
3
1
Liquid Crystal Group, Department of Physics, University of Gothenburg, Gothenburg, Sweden;
2
Faculty of Industrial Sciences and
Technology, University Malaysia Pahang, Kuantan, Malaysia;
3
Department of Chemistry and Industrial Chemistry, University of
Pisa, Pisa, Italy.
Email:
#
komitov@physics.gu.se, murthyhegde@gmail.com
Received November 16
th
, 2012; revised December 20
th
, 2012; accepted December 31
st
, 2012
ABSTRACT
Here we report on the study of vertical alignment of a nematic liquid crystal due to the segregation between perfluori-
nated and the polysiloxane groups of a multi-component composite alignment material. The measured surface anchor-
ing energy was found to depend on the relative amount of polysiloxane matrix in the composite material. These kind of
self-assembly will reduce the preparation time for display by eliminating few steps.
Keywords: VA; Nematic; Self Assembling; Vertical Alignment; Anchoring Energy
1. Introduction
Liquid Crystal alignment is the subject of interest ever
since it is used in the display industry. Many materials
capable to align liquid crystals (LC) have been discov-
ered lately and used for preparation of alignment layers
in liquid crystal displays (LCDs). Majority of these ma-
terials are devoted to vertical alignment (VA) since this
kind of alignment offers some advantages such as high
contrast ratio and no need for mechanical rubbing. The
most important physical mechanism behind VA is the
low surface energy of the alignment surface [1]. How-
ever, depending on the alignment material structure, the
LC molecules may interact sterically with the molecules
of the alignment material. As shown in ref. [2], the steric
interactions are playing an important role for the quality
of VA and the magnitude of the anchoring strength. Con-
siderable attention has been consecrated to self-assem-
bled materials, among all other materials which promote
VA, because of their wide applications in advanced ma-
terials such as optoelectronic materials since they have
the ability for self-assembling into regular manner with
Nano sized structures [3]. Perfluorinated groups are
widely used for many applications as self-assembled
materials since they show very interesting properties
such as low surface energy and high chemical and ther-
mal stability [3-7]. It has been observed that the align-
ment layers with low surface energy, such as the fluo-
rine-rich films, usually gives rise to VA since the surface
energy of the alignment layer is less than the surface en-
ergy of the liquid crystal [8,9]. In general fluorination
process enhances the rigidity of the molecules and in-
creases the stability by reinforcing the microphase seg-
regation with the polar groups due to the high electro-
negativity of the fluorine atoms [3,4,10]. In this work
perfluorinated groups, regarding their properties, were
used as a part of mixture to perform an alignment mate-
rial as a feasible method to achieve a uniform good VA
to fulfill LCDs development requirements.
2. Experimental
Here we report on the study of VA of a nematic liquid
crystal promoted by multi-component composite align-
ment materials. For our experimental study, conventional
sandwich cells were prepared. The cells’ substrates were
pre-coated with transparent conductive layer ITO with
alignment layer deposited on top of it.
A photopolymerized thin film, prepared from a mul-
ti-component composite material with perfluorinated and
polysiloxane groups as major components, was used as
alignment layer. The chemical structures of the compo-
nents of the composite alignment materials, which were
studied in this work, are shown in Figure 1.
The relative ratio of these components in the compos-
ite material blends are given in Table 1.
*
GH is thankful to the Universiti Malaysia Pahant for financial support
in the form of RDU grant RDU120367.
#
Corresponding author. Perfluorinated siloxane polymers have attracted our
Copyright © 2013 SciRes. SNL