International Journal of
Advanced Structures and Geotechnical Engineering
ISSN 2319-5347, Vol. 02, No. 01, January 2013
IJASGE 020103 Copyright © 2012 BASHA RESEARCH CENTRE. All rights reserved.
Mitigating Sulphate Attack in High Performance Concrete
BASHIR ALAM
1
, SALMAN AFZAL
2
, JUNAID AKBAR
1
, MUHAMMAD ASHRAF
3
,
KHAN SHAHZADA
1,
MUHAMMAD EJAZ SHABAB
4
1
Department of Civil Engineering, UET Peshawar, Pakistan
2
Department of Civil Engineering, IQRA National University, Peshawar, Pakistan
3
Department of Civil Engineering, CIIT, Abbottabad, Pakistan
4
Sarhad University of Science and Information Technology, Peshawar, Pakistan
Email: salmanafzalkhan@gmail.com
Abstract: The research addresses the mitigation of Sulphate attack on concrete as it is considered one of the
major degradation-causing phenomenons in the durability of concrete. The primary variable in the research was
the introduction of Silica Fume as a 12% replacement by weight of cement. Super-plasticizer was also used in
order to attain high strength and make the concrete more workable in the presence of silica fume. A concrete
batch, with a proper mix design was prepared, aiming at a high strength of 6000psi. Part of the batch was tested
for 28 days Strength and part of it was subjected to cyclic wetting and drying exposure to Sulphate-rich
environment, the solution being 50 g/l of Na
2
SO
4
. The quality of concrete was measured by Non-Destructive
Testing which showed an appreciable improvement in the resistance of concrete to Sulphate attack due to
addition of Silica fume whereas the Normal concrete cylinders were affected severely in the Sulphate
environment. The same concrete cylinders were tested afterwards for compressive strength under the Universal
Testing Machine and the results showed an alarming reduction in strength of the normal concrete cylinders
whereas the Silica fume made concrete cylinders showed small reduction in strength. The main conclusions
derived from this study are that the use of Silica fume leads to a better performance of concrete in Sulphate rich
environments although the strength may not be altered as desirable.
Keywords: Sulphate attack, Silica fume, Non-Destructive Testing, Universal Testing Machine
1. Introduction
Many concrete structures require costly repair works
as they deteriorate under the influence of aggressive
environmental agents. The most common among
these agents are alkali-aggregate reactivity, freeze-
thaw deterioration and attack by sulphates [1]. It is
for this reason that High-Performance Concrete has
been a choice of concrete mix designers for
achieving a long-lasting and economical structure
[2]. According to the Texas Department of
Transportation, sulphate attack is defined as a series
of reactions that may occur in hardened concrete
members as a result of presence of sulphate ions in
the matrix [3]. The products obtained from this
reaction hold a larger volume as compared to the
reactants in the cement matrix which causes an
internal stress generation propagated by the
expansion of the product. Ultimately, the concrete
will crack, spall and loss of mass occurs,
endangering the overall integrity of the design life of
the structure [4]. The United States Bureau of
Reclamations (USBR) was the pioneer of identifying
the sulphate attack in early 1908 and the only means
of mitigating this expansive reaction was controlling
the permeability of concrete [5]. The nature of the
manifestation of degradation due to sulphate attack
depends largely on several factors which include the
exposure conditions [6]. [7] has proposed a three-
kind exposure scenario for sulphate attack generation
i.e. continuous Immersion in sulphate environments,
cyclic exposure to wetting/ drying exposure in
sulphate environment and partial immersion in
sulphate environment. [8] determined that the cyclic
exposure to wetting/ drying in sulphate environment
leads to a strong scenario for degradation due to
sulphate attack and the time span is greatly reduced
for detecting the phenomenon.
One of the greatly debated agenda among
researchers remains as how to detect and quantify
the sulphate attack occurring in concrete members.
American Society for Testing and Materials has
developed a few tests for detecting deterioration due
to sulphate attack. [9] involves accelerating the
expansion of mortar which are cast in the form of
bars by the addition of gypsum to the Portland
cement. [10] is an immersion test of ASTM in which
mortar bars are immersed in 50 g/l sodium sulphate
solution and their expansion in monitored for a
period of six months. [11] has proposed an
experimental methodology for determining the
deterioration of concrete members due to sulphate
attack instead of cement mortar bars.
2. Materials and Methods
Materials:
Cement: ASTM Type-I cement (Normal cement)
was used during the study and by [12] the fineness of
cement was ensured.
Aggregates: The fine and coarse aggregate used in
the study was obtained from local quarries. Tests
were conducted on the aggregate specimen to collect