Desalination 144 (2002) 67–72
Presented at the International Congress on Membranes and Membrane Processes (ICOM), Toulouse, France,
July 7–12, 2002.
0011-9164/02/$– See front matter © 2002 Elsevier Science B.V. All rights reserved
*Corresponding author.
Molecular modelling of polyimide membranes
for gas separation
Matthias Heuchel*
a
, Dieter Hofmann
b
GKSS Research Center, Institute of Chemistry, Kantstrasse 55, D-14513 Teltow, Germany
a
Tel. +49 (3328)352-465;
b
Tel. +49 (3328) 352-247; Fax: +49(0)3328/352-452; emails: matthias.heuchel@gkss.de,
dieter.hofmann@gkss.de
Received 1 February 2002; accepted 15 February 2002
Abstract
Well-equilibrated molecular packing models have been produced for seven different polyimides. For all packings
the transport properties (solubility and diffusion coefficient) have been calculated for nitrogen, oxygen and carbon
dioxide using the Gusev-Suter method. Comparison with experimental data allowed to validate the quality of the
model structures. A significant improvement to former results could be assessed for the predicted selectivity values.
Keywords: Polyimide; Gas transport; Simulation; Solubility; Diffusion; Selectivity
1. Introduction
Polyimides (PIs) have attracted much attention
over the past years as material for gas separation
membranes [1–3]. Particular PIs synthesized from
2,2'-bis(3,4-dicarboxy-phenyl) hexafluoropropane
dianhydride (6FDA) show surprisingly high gas
selectivities for gas pairs as O
2
/N
2
and CO
2
/CH
4
.
Combined with high inherent chemical and thermal
stability as well as mechanical strength, these PIs
have been identified as promising materials for
applications, such as the recovery of H
2
from
industrial gas mixtures of CO
2
, N
2
or CH
4
, the
purification of natural gas and the enrichment of
either O
2
or N
2
from air.
One stimulus for the extensive research was
the observed tradeoff relationship between gas
permeability and permselectivity. Over the last 2
decades, intensive investigations have been per-
formed to study the structure property relation-
ships of polyimides by systematically changing
the diamine or dianhydride moieties [4–6]. Analysis
of this immense experimental material allowed