Two-stage crossover from thermal to quantum flux creep of dilute vortex ensembles in various high-T c superconducting thin films Johan J. A ˚ kerman Department of Materials Science-Tmfy-MSE, Royal Institute of Technology, S-100 44 Stockholm, Sweden and Physics Department, University of California—San Diego, 9500 Gilman Drive, La Jolla, California 92093-0319 E. L. Venturini and M. P. Siegal Sandia National Laboratories, Albuquerque, New Mexico 87185-1421 S. H. Yun and U. O. Karlsson Department of Materials Physics, Royal Institute of Technology, S-100 44 Stockholm, Sweden K. V. Rao Department of Materials Science-Tmfy-MSE, Royal Institute of Technology, S-100 44 Stockholm, Sweden Received 20 February 2001; published 8 August 2001 The thermal-to-quantum flux creep crossover at low vortex densities has been studied in YBa 2 Cu 3 O 7 , TlBa 2 CaCu 2 O 7- , and HgBa 2 CaCu 2 O 6+ thin films using ac susceptibility. The crossover temperatures T cr are 10–11, 17, and 30 K, respectively. Both thermal and quantum flux creep is suppressed as the vortex density is decreased. We observe a two-stage nature in the crossover behavior which appears to be a general property of all the three materials studied. DOI: 10.1103/PhysRevB.64.094509 PACS numbers: 74.60.Ge, 74.76.Bz I. INTRODUCTION Magnetic vortices in type-II superconductors are one of the few systems in which macroscopic quantum tunneling can occur. This intriguing phenomenon was first reported in high-T c superconductors HTS, 1 and although subsequently observed in conventional superconductors, 2–4 its study has mostly focused on optimally doped Y-123, 5–11 oxygen- deficient Y-123, 12,13 and other HTS materials such as Y 1 -x Pr x Ba 2 Cu 3 O 7 , 14 YBa 2 Cu 3 O 8 , 11 Bi 2 Sr 2 CaCu 2 O 8 , and Bi 2 Sr 2 Ca 2 Cu 3 O 10 , 15–17 Tl 2 Ba 2 CaCu 2 O 8 , 18–20 Tl 2 Ba 2 Ca 2 Cu 3 O 10 , 21 Hg 0.8 Tl 0.2 Ba 2 CaCu 3 O 8 , 22 and YBa 2 Cu 3 O 7 /PrBa 2 Cu 3 O 7 multilayers. 23,24 However, to the best of our knowledge, quantum creep has previously not been studied in either TlBa 2 CaCu 2 O 7 - Tl-1212or HgBa 2 CaCu 2 O 6 + Hg-1212, which are two of the materials investigated in this work. These material systems are of par- ticularly high technological importance due to their high critical temperature, high critical current density, and moder- ate anisotropy. 25,26 The low-temperature flux creep behavior can be very dif- ferent for single crystals and thin films of the same material. 27 The crossover temperature T cr , below which quantum creep effects can be observed, is generally higher for thin films. Theory also predicts a higher T cr in the case of single-vortex creep low fieldscompared to creep of flux bundles, since the tunneling probability decreases with the size of the tunneling object. 28 Thin films generally also show a strong suppression of quantum creep with decreasing field, whereas a similar anomaly is not observed for single crystals. This difference has been ascribed to differing characteristic pinning sites of thin films and single crystals. In particular it has been argued that the suppression of quantum creep as B 0 is due to the presence of a limited number of strong pinning sites that dominate the pinning at low vortex densi- ties. Hence, we expect both an increase in T cr and a decrease in overall creep in our thin film samples with highly dilute vortex ensembles. In this work we determine the thermal-to-quantum cross- over temperatures for Y-123, Tl- and Hg-1212 thin films at very low fields 7–140 Oe. While we find T cr =10– 11 K for Y-123 thin films, in good agreement with previously pub- lished high-field values, T cr is found to be as high as 17 and 30 K for Tl- and Hg-1212 thin films respectively. Further- more, the crossover seems to proceed in two distinct steps, and consequently a second temperature T cr * can be defined for all three materials. We also find that quantum creep is suppressed down to the lowest accessible fields. II. THERMAL AND QUANTUM CREEP The theory of collective flux creep 29,30 CFCpredicts a nonlinear current dependence of the flux creep activation en- ergy, UJ c = U 0 J c 0 J c -1 , 1 where J c 0 is the original critical current density before flux creep sets in, J c is the measured decaying critical current density and is an exponent describing the degree of non- linearity, with values between 1/7 and 5/2 depending on the actual collective flux creep regime. The concept of a temperature- and field-dependent exponent has been suc- cessfully applied in the analysis of flux creep in Y-123. 31–35 It is also well known that a simpler, logarithmic current dependence, 36 U ( J c ) =U 0 ln(J c0 /J c ), which formally corre- sponds to =0, is often a very good description of experi- PHYSICAL REVIEW B, VOLUME 64, 094509 0163-1829/2001/649/0945095/$20.00 ©2001 The American Physical Society 64 094509-1