ISSN 1063-7834, Physics of the Solid State, 2013, Vol. 55, No. 11, pp. 2229–2233. © Pleiades Publishing, Ltd., 2013.
Original Russian Text © A.D. Bouravleuv, N.V. Sibirev, D.V. Beznasyuk, N. Lebedeva, S. Novikov, H. Lipsanen, G.E. Cirlin, 2013, published in Fizika Tverdogo Tela, 2013,
Vol. 55, No. 11, pp. 2118–2122.
2229
1. INTRODUCTION
Recently, quasi-one-dimensional nanostructures
such as nanowhiskers (NW) are of great interest due to
not only their many-sided properties, but also a variety
of their potential applications. It was shown up to now
that almost all existing devices of semiconductor
nano- and optoelectronics such as transistors, photo-
electric transducers, lasers, biosensors, and so on can
be developed on the basis of NW. Owing to their sizes
and unique shape, NW are also promising objects for
designing micro- and nanoelectromechanical sensors,
pickups, and other similar devices. However, the mea-
surement of the mechanical properties of individual
NW is a certain problem because of complexity related
to the application of standard techniques [1]. Never-
theless, various methods of determining the mechani-
cal properties of NW based on both the excitation of
mechanical vibrations during applying electric field
and the use of atomic-force microscopy (AFM) have
already been proposed. For example, the Young’s
moduli of SiC [2] and GaAs [3] nanowhiskers were
determined during their elastic bending under pres-
sure of an AFM probe with simultaneous measure-
ment of the loading–unloading dependences. In turn,
the parameters of mechanical vibrations of boron-
based NW were found using a scanning electron
microscope (SEM) [4, 5]. The excitation of vibrations
in NW pinned at the AFM probe tip was performed
both mechanically by applying a stress immediately to
the probe and by applying ac electric field between the
AFM probe and an additional electrode located near
the NW. Similar technique based on the excitation of
vibrations by ac electric field was also used for studying
the properties of GaN [6], ZnO [7], SiC [8, 9], and
SiO
2
[10] nanowhiskers.
This work is devoted to a new method of determin-
ing the Young’s modulus of (Ga,Mn)As NW based on
the excitation and immediate measurement of their
mechanical vibrations using a scanning electron
microscope.
2. METHODS
(Ga,Mn)As NW were grown in a VG100H molec-
ular-beam epitaxy device. The growth processes were
described in detail in [11]. The synthesis was per-
formed on GaAs substrates with the (111)B-type crys-
tallographic orientation at the growth temperature T =
660°C.
The surface morphology of the samples prepared
was studied by scanning electron microscopy on a
Zeiss Supra 40 microscope.
3. RESULTS AND DISCUSSION
The SEM study of the morphology of NW arrays
grown by molecular-beam epitaxy revealed that the
NW images are smeared at certain scanning rates. The
detailed study of positions of specific (Ga,Mn)As NW
showed that NW vibrate (Fig. 1). The displacement of
the SEM beam during the image scanning can lead to
charging–discharging of the NW tip and, as a result, to
the Coulomb interaction between NW and the elec-
tron beam. In this case, the NW vibrations can be gen-
SEMICONDUCTORS
New Method of Determining the Young’s Modulus of (Ga,Mn)As
Nanowhiskers with a Scanning Electron Microscope
A. D. Bouravleuv
a, b, c,
*, N. V. Sibirev
a, b
, D. V. Beznasyuk
a, b
, N. Lebedeva
d
,
S. Novikov
d
, H. Lipsanen
d
, and G. E. Cirlin
a–c
a
St. Petersburg Academic University, ul. Khlopina 8/3, St. Petersburg, 194021 Russia
b
Ioffe Physical-Technical Institute, Russian Academy of Sciences,
Politekhnicheskaya ul. 26, St. Petersburg, 194021 Russia
* e-mail: bour@mail.ioffe.ru
c
Institute for Analytical Instrumentation, Russian Academy of Sciences,
Rizhskii pr. 26, St. Petersburg, 198103, Russia
d
Aalto University, Värmemansgränden 2, Espoo, 02150 Finland
Received April 10, 2013
Abstract—Arrays of (Ga,Mn)As nanowhiskers have been grown by molecular-beam epitaxy. The scanning
electron microscopy study of the surface morphology of the samples has revealed the appearance of mechan-
ical vibrations of individual nanowhiskers. To describe the vibrations, a model has been developed for the
determination of the Young’s modulus of (Ga,Mn)As nanowhiskers.
DOI: 10.1134/S1063783413110061