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Although the kinetics of CF formation/
dissolution is still unclear, it is widely
accepted that the CF formation/dissolu-
tion is strongly related to the electromigra-
tion and electrochemical reaction of anion
(i.e., oxygen vacancy)
[13–16]
or cation (i.e.,
Cu
2+
, Ag
+
or Ni
2+
).
[17–22]
Generally, RS behavior can be classi-
fied as two modes: nonvolatile memory
switching (MS) and volatile threshold
switching (TS). In the MS mode, both
LRS and HRS can be maintained after
removing the external voltage, while the
LRS in the TS mode will be back to the
HRS once the applied voltage is smaller
than a critical value.
[23–25]
To avoid confu-
sion with MS, the LRS and HRS in TS are
renamed as “TS ON-state” and “TS OFF-
state” in this article. The MS device can be
used for the non-volatile data storage
[1–5]
while TS device can be as a selector in
series with memory cell to suppress
crosstalk effect in the crossbar array.
[26–30]
Recently, some groups reported that TS
and MS can coexist and mutually transform in a single device
at suitable external excitation.
[23–28]
Several models have been
proposed to explain this phenomenon, including CF thermal
instability,
[23]
strong electron correlation effect,
[24]
quantum-wire
model,
[25]
interface barrier modulation,
[26]
and space charge
effect.
[27]
However, the underlying mechanism of the phenom-
enon is still unclear, especially lacking of direct evidences to
uncover when and how the two RS modes happen and what is
the internal relationship between them.
Here, we demonstrate that the TS and MS modes can be
modulated in the Ag/SiO
2
/Pt structure by controlling the com-
pliance current ( I
CC
) in electroforming. We systematically inves-
tigate the morphologies, chemical components, and dynamic
growth of the CF using scanning electron microscope (SEM),
high-resolution transmission electron microscopy (HRTEM)
and electron energy loss spectroscopy (EELS) analysis. The
results confirm that the TS and MS modes correspond to the
CF consisting of isolated and continuous Ag nanocrystals,
respectively. In addition, by Kelvin probe force microscopy
(KPFM) studies, the voltage potential distribution of CF in
the ON- and OFF-state further indicate that the TS mode is
Direct Observation of Conversion Between Threshold
Switching and Memory Switching Induced by Conductive
Filament Morphology
Haitao Sun, Qi Liu,* Congfei Li, Shibing Long, Hangbing Lv, Chong Bi, Zongliang Huo,
Ling Li, and Ming Liu*
Volatile threshold switching (TS) and non-volatile memory switching (MS)
are two typical resistive switching (RS) phenomena in oxides, which could
form the basis for memory, analog circuits, and neuromorphic applications.
Interestingly, TS and MS can be coexistent and converted in a single device
under the suitable external excitation. However, the origin of the transition
from TS to MS is still unclear due to the lack of direct experimental evidence.
Here, conversion between TS and MS induced by conductive filament (CF)
morphology in Ag/SiO
2
/Pt device is directly observed using scanning electron
microscopy and high-resolution transmission electron microscopy. The MS
mechanism is related to the formation and dissolution of CF consisting of
continuous Ag nanocrystals. The TS originates from discontinuous CF with
isolated Ag nanocrystals. The results of current–voltage fitting and Kelvin
probe force microscopy further indicate that the TS mechanism is related to
the modulation of the tunneling barrier between Ag nanocrystals in CF. This
work provides clearly experimental evidence to deepen understanding of the
mechanism for RS in oxide-electrolyte-based resistive switching memory,
contributing to better control of the two RS behaviors to establish high-perfor-
mance emerging devices.
DOI: 10.1002/adfm.201401304
H. Sun, Dr. Q. Liu, C. Li, Dr. S. Long, Dr. H. Lv,
Dr. C. Bi, Prof. Z. Huo, Prof. L. Li, Prof. M. Liu
Lab of Nanofabrication and Novel Device Integration
Institute of Microelectronics
Chinese Academy of Sciences
Beijing 100029, China
E-mail: liuqi@ime.ac.cn; liuming@ime.ac.cn
1. Introduction
Resistive switching (RS) phenomenon induced by redox in
oxide electrolyte provides attractive prospects for resistive
random access memory (RRAM), analog circuits and other
neuromorphic applications.
[1–5]
Due to simple structure, high
speed, low power and excellent scalability, the redox-based
RRAM is very suitable for 3D ultrahigh density storage.
[6–12]
Under external electrical stimulations, the resistance of the
RRAM cell can be switched between high resistive state (HRS)
and low resistive state (LRS) due to the formation/dissolution
of conductive filament (CF) inside the insulator layer.
[13–22]
Adv. Funct. Mater. 2014,
DOI: 10.1002/adfm.201401304
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