Completely Biodegradable Composites of Poly(propylene
carbonate) and Short, Lignocellulose Fiber Hildegardia
populifolia
X. H. LI,
1
Y. Z. MENG,
1,3
S. J. WANG,
1
A. VARADA RAJULU,
4
S. C. TJONG
2
1
Guangzhou Institute of Chemistry, Chinese Academy of Sciences, P.O. Box 1122, Guangzhou 510650, China
2
Department of Physics and Materials Sciences, City University of Hong Kong, 83 Tat Chee Avenue,
Kowloon, Hong Kong
3
Institute of Energy and Environment Materials, School of Physics and Engineering, Sun Yat-Sen University,
Guangzhou 510275, China
4
Department of Polymer Science and Technology, S.K. University, Anantapur-515003, India
Received 27 November 2002; revised 29 September 2003; accepted 6 October 2003
ABSTRACT: The composites of biodegradable poly(propylene carbonate) (PPC) rein-
forced with short Hildegardia populifolia natural fiber were prepared by melt mixing
followed by compression molding. The mechanical properties, thermal properties, and
morphologies of the composites were studied via static and dynamic mechanical mea-
surements, thermogravimetric analysis, and scanning electron microscopy (SEM) tech-
niques, respectively. Static tensile tests showed that the stiffness and tensile strength
of the composites increased with an increasing fiber content. However, the elongation
at break and the energy to break decreased dramatically with the addition of short
fiber. The relationship between the experimental results and the compatibility or
interaction between the PPC matrix and fiber was correlated. SEM observations indi-
cated good interfacial contact between the short fiber and PPC matrix. Thermogravi-
metric analysis revealed that the introduction of short Hildegardia populifolia fiber led
to a slightly improved thermooxidative stability of PPC. © 2004 Wiley Periodicals, Inc. J
Polym Sci Part B: Polym Phys 42: 666 – 675, 2004
Keywords: composites; polycarbonates; natural fiber; mechanical properties; biode-
gradable
INTRODUCTION
Biodegradable plastics such as aliphatic polyes-
ter, cellulose-based thermoplastics, and other po-
lysaccharide-based plastics have attracted much
attention in recent years from the point of view of
environmental protection.
1,2
Most of the biode-
gradable plastics, for example, the aliphatic poly-
esters including poly(3-hydroxy-butyrate-co-3-hy-
droxyvalerate) and poly(butylenes succinate),
have poor mechanical strength and modulis than
those of commercial thermoplastics.
3–8
Fiber re-
inforcement is an effective way to improve the
mechanical properties of thermoplastics. How-
ever, conventional reinforcing materials such as
glass fiber, carbon fiber, and aramid fiber are
nondegradable and difficult to incinerate. In this
Correspondence to: Y. Z. Meng, Guangzhou Institute of
Chemistry, Chinese Academy of Sciences, P. O. Box 1122,
Guangzhou 510650, China (E-mail: mengyz@yahoo.com)
Journal of Polymer Science: Part B: Polymer Physics, Vol. 42, 666 – 675 (2004)
© 2004 Wiley Periodicals, Inc.
666