93
Am. J. Enol. Vitic. 60:1 (2009)
The visual characteristic of red wine is mainly due to
anthocyanins that are present in the grape skin at harvest
and that dissolve in the red wine during the maceration/
fermentation process (Amrani Joutei and Glories 1995,
Romero-Cascales et al. 2005a). Anthocyanins accumu-
late gradually in berry skins during ripening (Fernán-
dez-López et al. 1992), and their total amount at harvest
depends on variety (i.e., pink, red, or black skin variety)
and many other factors, including environmental param-
eters and agronomic practice (Guidoni et al. 2008). The
types and the amounts of various anthocyanins in grape
skins (their “profile”) determine the color of resulting
wines, but their extraction from the grape skin into the
wine depends on the tendency of the berry skin to release
them (González-Neves et al. 2004, Romero-Cascales et
al. 2005b). The extractability of anthocyanins increases
throughout grape ripening as a consequence of cell wall
degradation by pectolytic enzymes (Ribéreau-Gayon et
al. 2000). Differences in polysaccharides based on galac-
tose and arabinose, the cellulose content, and the degree
of methylation of the pectins could be responsible for the
difference in anthocyanin extractability (Ortega-Regules
et al. 2006, 2008).
Several studies have attempted to define the best
method to evaluate polyphenolic compounds in grapes
and their ease of release. These analytical methods are
generally rather complex and often require long analysis
times (Cagnasso et al. 2008). Furthermore, some data in-
terpretation may be difficult (Venencie et al. 1998).
Texture analysis is a current analytical technique used
for measurement of the physical properties of food. For
winegrapes, the literature contains studies on modifica-
tions of some grape textural properties during ripeness
(Abbal et al. 1992, Robin et al. 1997, Lee and Bourne
1980, Grotte et al. 2001) and the influence of climate and
growing location on mechanical behavior (Le Moigne et
al. 2008).
The aim of this work was to examine the relation-
ship between skin hardness, determined by puncture test,
and the ease of extractability of anthocyanins in berries
at different ripening stages. The study was carried out
on Brachetto, an important aromatic red grape variety
used for production of sweet sparkling wines (6–7.5%
vol ethanol) and grown in Piedmont (northwest Italy).
The ease and rapidity of extraction are important qualita-
tive parameters for Brachetto grapes. These aromatic red
grapes are subjected to very short fermentation-macera-
tion (24–48 hr) because the product obtained must not
exceed 3.5% vol ethanol before the second fermentation
( prise de mousse). Reduced maceration times, low fer-
mentation temperature (17–18°C) to preserve aromatic
components, and low alcohol concentrations frequently
lead to reduced pigment extraction and wines with un-
satisfactory color. Knowledge of the extractability of an-
thocyanin compounds measured via berry skin hardness
could permit harvesting at an optimal stage of ripeness
and suitable operative choices in the prefermentation and
maceration phases.
1
Researcher,
2
Ph.D. student,
3
Professor, Di.Va.P.R.A., Microbiology and Food
Technology sector, University of Turin, Via L. da Vinci 44, 10095 Grugliasco,
Torino, Italy.
*Corresponding author (email: luca.rolle@unito.it; tel: 39 0116708558; fax:
39 0116708549)
Acknowledgment: This study was funded by Consorzio Tutela Vini d’Acqui,
Brachetto d’Acqui.
Manuscript submitted May 2008, revised July 2008, accepted Sept 2008.
Publication costs of this article defrayed in part by page fees.
Copyright © 2009 by the American Society for Enology and Viticulture. All
rights reserved.
Research Note
Relationship between Skin Break Force and Anthocyanin
Extractability at Different Ripening Stages
Luca Rolle,
1
* Fabrizio Torchio,
2
Giuseppe Zeppa,
1
and Vincenzo Gerbi
3
Abstract: The extractability of anthocyanins from winegrapes with different skin hardness at two different
ripening stages was evaluated. Skin hardness was assessed by texture analysis, a rapid and low-cost analytical
technique. Grape berries of cv. Brachetto were calibrated according to their density estimated by flotation in 10
different salt solutions. Skin hardness was measured via a puncture test, and two groups of berries with different
skin hardness were selected for each ripening stage: soft (<0.40 N) and hard (>0.50 N). Anthocyanin skin extrac-
tion was evaluated in a hydroalcoholic model solution and the kinetics of skin dissolution was monitored. For each
ripening stage, the harder skin had greater anthocyanin extractability. Significant interactions between ripening
stage and skin hardness were found in the composition of individual anthocyanins present in the extract.
Key words: extractability, anthocyanin, skin hardness, texture analysis, puncture test