TECHNICAL REPORTS
794
Elucidating veterinary antibiotic interactions with soil is important
for assessing and mitigating possible environmental hazards. he
objectives of this study were to investigate the efects of vegetative
management, soil properties, and >1000 Da dissolved organic matter
(DOM
>1000 Da
) on sulfamethazine (SMZ) behavior in soil. Sorption
experiments were performed over a range of SMZ concentrations
(2.5–50 μmol L
-1
) using samples from three soils (Armstrong,
Huntington, and Menfro), each planted to one of three vegetation
treatments: agroforestry bufers strips (ABS), grass bufer strips
(GBS), and row crops (RC). Our results show that SMZ sorption
isotherms are well itted by the Freundlich isotherm model (log
K
f
= 0.44–0.93; Freundlich nonlinearity parameter = 0.59–0.79).
Further investigation of solid-to-solution distribution coeicients
(K
d
) demonstrated that vegetative management signiicantly (p <
0.05) inluences SMZ sorption (ABS > GBS > RC). Multiple linear
regression analyses indicated that organic carbon (OC) content,
pH, and initial SMZ concentration were important properties
controlling SMZ sorption. Study of the two most contrasting soils
in our sample set revealed that increasing solution pH (pH 6.0–
7.5) reduced SMZ sorption to the Armstrong GBS soil, but little
pH efect was observed for the Huntington GBS soil containing
50% kaolinite in the clay fraction. he presence of DOM
>1000 Da
(150 mg L
-1
OC) had little signiicant efect on the Freundlich
nonlinearity parameter; however, DOM
>1000 Da
slightly reduced
SMZ K
d
values overall. Our results support the use of vegetative
bufers to mitigate veterinary antibiotic loss from agroecosystems,
provide guidance for properly managing vegetative bufer strips
to increase SMZ sorption, and enhance understanding of SMZ
sorption to soil.
Sulfamethazine Sorption to Soil: Vegetative Management, pH,
and Dissolved Organic Matter Efects
Bei Chu, Keith W. Goyne,* Stephen H. Anderson, Chung-Ho Lin, and Robert N. Lerch
S
ulfamethazine (4-amino-N-[4, 6-dimethyl-2-py-
rimidinyl] benzenesulfonamide) (SMZ) is one of the sul-
fonamide veterinary antibiotics (VAs) commonly used for
livestock and aquaculture disease treatment, disease prevention,
and growth promotion (Sarmah et al., 2006). In the United
States, approximately 3.63 × 10
5
kg of SMZ is used annually as
a feed additive for cattle and swine production (Mellon et al.,
2001). Like most VAs, SMZ is poorly absorbed and metabo-
lized ater entering a human or animal body, and the typical
SMZ concentration in manure and manure slurry is on the order
of 3 to 35 μmol kg
-1
(Haller et al., 2002; Kumar et al., 2005;
Burkhardt et al., 2005; Shelver et al., 2010). Sulfamethazine
concentrations in soil fertilized with manure range from non-
detectable to several micromoles per kilogram (Hamscher et al.,
2005; Aust et al., 2008). In surface runof from manured plots,
SMZ concentrations can reach 2.5 to 6.8 μmol L
-1
(Burkhardt
et al., 2005; Kreuzig et al., 2005). Additionally, 1 to 4% of the
initial quantity of sulfonamides applied to test plots can be lost
via short (<100 min) surface runof events (Burkhardt et al.,
2005; Kreuzig et al., 2005).
In some cases, VA inputs to soil may afect the quantity and
quality of native microbial communities (Kotzerke et al., 2008;
Kümmerer, 2003; Nygaard et al., 1992; Westergaard et al.,
2001). Although VA concentrations are very low in most soils,
they may lead to the increased selection pressure of VA-resistant
bacteria in the environment (Kümmerer, 2003; Nygaard et al.,
1992). Land application of manure is a primary source of VA
release into the environment, resulting in the development of
antibiotic-resistant genes within microorganisms (Aarestrup
and Wegener, 1999; Herron et al., 1998; Nygaard et al., 1992).
For example, multiple tetracycline- and sulfonamide-resistant
genes were detected in dairy lagoon water, irrigation ditch water,
and urban/agriculturally impacted river sediment samples from
northern Colorado (Pruden et al., 2006). Spreading of antibiotic-
resistant genes causes public concern that human pathogens will
develop antibiotic resistance and be diicult to treat with current
antibiotics (Shea, 2003). An additional concern is that SMZ and
Abbreviations: ABS, agroforestry bufers strip; CBD, citrate–bicarbonate–
dithionite; DOM, dissolved organic matter; GBS, grass bufer strip; HPLC, High-
performance liquid chromatography; OC, organic carbon; RC, row crop; SMZ,
sulfamethazine; VA, veterinary antibiotic.
B. Chu, K.W. Goyne, and S.H. Anderson, Dep. of Soil, Environmental and Atmospheric
Sciences, Univ. of Missouri, 302 ABNR Building, Columbia, MO 65211; C.-H. Lin,
Center for Agroforestry, Univ. of Missouri, 203 ABNR Building, Columbia, MO 65211;
R.N. Lerch, USDA–ARS, Cropping Systems and Water Quality Research Unit, 269 Ag.
Eng. Bldg., Columbia, MO 65211. Assigned to Associate Editor K.G. Karthikeyan.
Copyright © American Society of Agronomy, Crop Science Society of America,
and Soil Science Society of America. 5585 Guilford Rd., Madison, WI 53711 USA.
All rights reserved. No part of this periodical may be reproduced or transmitted
in any form or by any means, electronic or mechanical, including photocopying,
recording, or any information storage and retrieval system, without permission in
writing from the publisher.
J. Environ. Qual. 42:794–805 (2013)
doi:10.2134/jeq2012.0222
Supplemental data ile is available online for this article.
Received 30 May 2012.
*Corresponding author (goynek@missouri.edu).
Journal of Environmental Quality
ORGANIC COMPOUNDS IN THE ENVIRONMENT
TECHNICAL REPORTS