Anodic Aluminum Oxide Templated Channel Electrodes via Atomic Layer
Deposition
A. B. F. Martinson
a,b
, J. W. Elam
b
, J. T. Hupp
*,a
, M. J. Pellin
b
a
Department of Chemistry, Northwestern University, Evanston, Illinois 60208, USA
b
Argonne National Lab, Division of Materials Science, Argonne, Illinois 60439, USA
Dye-sensitized solar cells (DSSCs) utilize high surface area metal
oxide sintered particle networks to absorb molecular dyes and
transport injected charge carriers. While this sintered particle
architecture allows liquid electrolyte DSSCs to achieve efficiencies
up to 11%, slow charge transport through the semiconductor
network limits the amount of modification that can be made to the
electrolyte and dye without adversely affecting the efficiency. The
functionalization of anodic aluminum oxide membranes with thin
films of transparent, semiconducting oxides via atomic layer
deposition may allow for significantly faster charge transport. We
demonstrate the fabrication of ZnO thin films within and upon
commercially available anodic aluminum oxide membranes via
atomic layer deposition.
Introduction
Dye sensitized solar cells (DSSCs) comprise an increasingly attractive alternative
energy conversion technology.(1, 2) These photoelectrochemical cells use molecular dyes
to sensitize high area, wide band gap semiconductor oxide photoanodes. Typically, a
liquid electrolyte based on iodide/triiodide scavenges the hole left on the dye and shuttles
it to a Pt-coated counter electrode where the circuit is completed. Solid-state (molecular
or polymeric) hole scavenger/conductor have also been used.(2) The most efficient
DSSCs convert AM1.5 solar insolation to electrical energy with 11% efficiency, but
suffer from relatively poor photovoltages due to the overpotential needed to drive the dye
regeneration reaction. Furthermore, they show less than optimal photocurrents due to
insufficient light collection at wavelengths > 700 nm.(3)
Compared to the most efficient nanocrystalline TiO
2
photoanodes, devices fabricated
with ZnO electrodes show significantly lower conversion efficiencies (4%).(4-6) Despite
superior recombination dynamics, poor dye loading and charge injection into ZnO reduce
the total photocurrent yield.(7) Yet ZnO DSSCs continue to be actively investigated due
to the ease with which alternative and potentially superior high-area semiconductor
morphologies may be fabricated. Particularly interesting are nominally 1-D arrays.
Compared with standard photoanodes based on sintered nanocrystalline particles, 1-D
photoanodes should show significantly faster electron transport, owing to a more direct
path to the conductive glass electrode combined with fewer sites for trapping electrons.
To this end, several novel photoanode architectures have been fabricated, including but
not limited to hydrothermally grown ZnO nanorod arrays, electrodeposited ZnO platelets,
and TiO
2
pores formed via titanium anodization.(8-10) In the most successful application
of this idea to date, a 1.5% efficient ZnO nanorod array has been shown to exhibit
significantly faster transport compared to nanoparticle networks.(11, 12) The efficiency
ECS Transactions, 6 (25) 389-394 (2008)
10.1149/1.2943259, ©The Electrochemical Society
389
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