Introduction
In recent years, the plastic materials have became an
important part of solid urban waste, with plastics from
containers and packaging representing around 60% of
this type of waste. The composition of this residue is
mainly polyolefins (high and low density polyethyl-
ene, polypropylene and polystyrene), accounting for
around 70% of the total plastic waste [1]. As only a
small amount of waste plastic is recycled and most
plastics are not biodegradable, these strong uses have
led to the generation of an increased amount of plastic
waste. Therefore, technical have to be implemented to
reduce plastic wastes negative impact on the environ-
ment. Landfilling or incineration of plastic waste are
not the right solutions, because the former has the
danger of leaching and soil impregnation of its degra-
dation products and the latter produce several pollut-
ants (nitrous and sulphur oxides, dusts, dioxins and
other toxins) that have a highly negative impact on
the environment. Both processes do not allow the re-
covery of the organic content of plastic waste, which
should be part of the organic life-cycle.
The search for new alternative fuels, together
with the necessity of searching new technology to re-
duce the negative environment impact of plastic
wastes, has led to the idea of studying co-pyrolysis of
plastic wastes and oil shale.
The plastics consist of hydrocarbons-type
macromolecules with a significant intrinsic energy and a
very high calorific value [2, 3]. These materials are rich
in hydrogen in comparison with coal [4, 5–9] and oil
shale [10–15]. Oil shale, on the other hand, is consid-
ered to be the substitute for oil as a natural source of en-
ergy. However, the extraction of oil from oil shale is rel-
atively expensive and uneconomical. Therefore, re-
search for processes of oil shale utilization as a source of
energy gains a high level of importance [16–19].
The three oil shale deposits in Morocco (Timahdit,
Tanger and Tarfaya) represent about 15% of known oil
shale resources in the world [20]. Extensive exploration
and processing research has been conducted over the
past decades [21]. These shale oil resources have been
estimated to be 50 billion barrels [20]. Timahdit and
Tarfaya oil shale deposits are the biggest and the most
explored deposits in Morocco to have the potential to
yield 17 and 23 billion barrels respectively.
The co-treatment of oil shale mixed with plastic
wastes into useful energetic products or into valuable
chemicals can be achieved in a thermochemical pro-
cesses [10–15]. Pyrolysis has received special atten-
tion since it produces solid, liquid and gas products.
With these purposes, the knowledge of the kinetics of
degradation is necessary for the design of specific re-
actors. Thermogravimetric behaviour has been
proved to be a very powerful tool for materials char-
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Journal of Thermal Analysis and Calorimetry, Vol. 89 (2007) 1, 203–209
PYROLYSIS KINETICS OF POLYPROPYLENE
Morocco oil shale and their mixture
A. Aboulkas
1
, K. El Harfi
1*
, A. El Bouadili
2
, M. Ben Chanâa
1
and A. Mokhlisse
1
1
Laboratoire de Chimie Physique, Département de Chimie, Faculté des Sciences Semlalia, Université Caddi Ayyad, BP 2390,
40001 Marrakech, Maroc
2
Laboratoire de Chimie Organique et Analytique, Departément de Chimie, Faculté des Sciences et Techniques de Béni-Mellal,
Université Caddi Ayyad, BP 523, 23000 Béni-Mellal, Maroc
The pyrolysis of oil shale and plastic wastes is being presently considered as an alternative means of partial substitution of fossil fu-
els to generate the necessary energy to supply the increasing energy demand and as well as new technology to reduce the negative
environment of plastic wastes. However, Knowledge of pyrolysis kinetics is of great imponrtance for the design and simulation of
the reactor and in order to establish the optimum process conditions.
In this study, the thermal decomposition of polypropylene, oil shale and their mixture was studied by TG under a nitrogen at-
mosphere. Experiments were carried out for various heating rates (2, 10, 20, 50 K min
–1
) in the temperature range 300–1273 K. The
values of the obtained activation energies are 207 kJ mol
–1
for polyethylene, 57 kJ mol
–1
for the organic matter contained in the oil
shale and 174 kJ mol
–1
for the mixture. The results indicate that the decomposition of these materials depends on the heating rate,
and that polypropylene acts as catalyst in the degradation of the oil shale in the mixture.
Keywords: dynamic thermogravimetry, kinetics, oil shale, polypropylene, pyrolysis
* Author for correspondence: elharfi@ucam.ac.ma