EXTRACTION AND CHARACTERIZATION OF POLYPHENOL
OXIDASE IN PAWPAW (ASIMINA TRILOBA) FRUIT
CAODI FANG
1
, CHANGZHENG WANG
3
, YOULING L. XIONG
1,2,5
and
KIRK W. POMPER
4
1
Graduate Center for Nutritional Sciences
2
Department of Animal and Food Sciences
University of Kentucky
Lexington, KY 40546
3
Human Nutrition Program
4
Horticultural Research Program
Kentucky State University
Frankfort, KY 40601
Accepted for Publication November 10, 2006
ABSTRACT
Crude polyphenol oxidase (PPO) was extracted from pawpaw (Asimina
triloba) fruit pulp, partially purified by gel filtration and electrophoresed for
molecular weight (MW) determination. The enzyme activity was assayed by
monitoring the absorbance (420 nm) of the PPO extract-catechol mixtures
over time. The PPO activity varied with pH and was the greatest at pH
6.5–7.0. The crude enzyme exhibited a maximum activity at 5–20C, but a brief
exposure to 40–80C resulted in a rapid decline or complete loss of the enzyme
activity. The enzyme kinetics based on the reaction rate in the linear region
(0–60 s) showed a V
max
of 0.1363/s and a K
m
of 0.3266 M for the crude PPO.
The PPO existed as two isoforms with MWs of 28.2 and 38.3 kDa, respectively.
PRACTICAL APPLICATIONS
Pawpaw fruit is a low-acid, sweet and aromatic fruit grown in North
America. With its intense flavor resembling a combination of banana, mango
and pineapple, pawpaw fruit is being used in value-added products such
as ice creams, yogurts and baked foods. However, pawpaw fruit has a short
5
Corresponding author. TEL: (859) 257-3822; FAX: (859) 257-5318; EMAIL: ylxiong@uky.edu
Journal of Food Biochemistry 31 (2007) 603–620. All Rights Reserved.
© 2007, The Author(s)
Journal compilation © 2007, Blackwell Publishing
603