e506 VOLUME 38 • NUMBER 8 • SEPTEMBER 2007
QUINTESSENCE INTERNATIONAL
During the last decade, the use of titanium
for cast restorations, such as resin-bonded
fixed partial dentures and implant-supported
prostheses, has increased substantially.
1–3
Despite the development of new-generation
casting machines and investment materials,
several problems persist.
1,4,5
One of the prob-
lems associated with titanium castings is
insufficient bonding between titanium metal
frameworks and veneering materials and lut-
ing agents, which has impeded the achieve-
ment of favorable clinical results.
5,6
Cast titanium has a great clinical applica-
bility due to its favorable and innumerous
characteristics. It has excellent biocompatibil-
ity, high corrosion resistance, low density,
and a high strength/weight ratio. Several
studies have, therefore, attempted to optimize
the efficacy of the chemical bond systems for
binding resin to titanium, keeping in mind
that composite materials can be bonded to
Effect of metal conditioners on the adhesive
bonding of resin cements to cast titanium
Sicknan Soares da Rocha, DDS MSc, PhD
1
/
Gelson Luis Adabo, DDS, MSc, PhD
2
/
Sandra Gouveia Spinola, DDS
3
/
Renata Garcia Fonseca, DDS, MSc, PhD
4
/
Anelise Rodolfo Ferreira, DDS, MSc
5
Objective: To assess the effect of metal conditioners on the bond strength between resin
cements and cast titanium. Method and Materials: Commercially pure titanium (99.56%)
was cast using an arc casting machine. Surfaces were finished with 400-grit silicon car-
bide paper followed by air abrasion with 50-µm aluminum oxide. A piece of double-coated
tape with a 4-mm circular hole was then positioned on the metal surface to control the
area of the bond. The prepared surfaces were then divided into 4 groups (n=10): G1,
unprimed Panavia F; G2, Alloy Primer–Panavia F; G3, unprimed Bistite DC; G4, Metaltite-
Bistite DC. Forty minutes after insertion of the resin cements, the specimens were
detached from the mold and stored in water at 37°C for 24 hours. Shear bond strength
was performed in a testing machine (MTS 810) at a crosshead speed of 0.5 mm/min.
Data were analyzed using ANOVA and Tukey’s test with a .05 significance level. The frac-
tured surfaces were observed through an optical microscope at 10 magnification.
Results: The G1 group demonstrated significantly higher shear bond strength (17.95
MPa) than the other groups. G3 (13.79 MPa) and G4 (12.98 MPa) showed similar mean
values to each other and were statistically superior to G2 (9.31 MPa). Debonded surfaces
generally presented adhesive failure between metal surfaces and resin cements.
Conclusion: While the Metaltite conditioner did not influence the bond strength of the
Bistite DC cement, the Alloy Primer conditioner significantly decreased the mean bond
strength of the Panavia F cement. (Quintessence Int 2007;38:709.e506-510)
Key words: fixed partial denture, metal conditioners, resin cements, shear bond strength,
titanium
1
Professor, Health Science Institut, Paulista University (UNIP),
Goiânia, GO, Brazil.
2
Associate Professor, Department of Dental Materials and
Prosthodontics, São Paolo State University (UNESP),
Araraquara Dental School, Araraquara, SP, Brazil.
3
Postgraduate Student, São Paolo State University (UNESP),
Araraquara Dental School, Araraquara, SP, Brazil.
4
Assistant Professor, Department of Dental Materials and
Prosthodontics, São Paolo State University (UNESP),
Araraquara Dental School, Araraquara, SP, Brazil.
5
Postgraduate Student, Department of Dental Materials and
Prosthodontics, São Paolo State University (UNESP), Araraquara
Dental School, Araraquara, SP, Brazil.
Correspondence: Dr Gelson Luis Adabo, Department of Dental
Materials and Prosthodontics, São Paolo State University
(UNESP), Rua Humaitá, 1680-CEP: 14801-903. CP: 331,
Araraquara, SP, Brazil. Fax: 55 (16) 201-6406. E-mail: adabo@
foar.unesp.br
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