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in terms of the first two attributes,
the stability of these devices remains
unproven.
[1–3]
For solid-state dye sensitized
(ssDSSC)
[4]
and perovskite sensitized
solar cells (PSSC)
[5]
non-stoichiometry
induced defects in TiO
2
appears to be a
limiting factor for two of the key param-
eters; efficiency and more importantly
the long-term photo-stability. Limitation
in charge transport is an important factor
for device performance, which has been
studied extensively in context of ssDSSCs.
Recently the emergence of perovskite-
based solar cells (PSSCs) has led to a
marked increase in solid-state device per-
formance, to up to 15%. In the perovskite
devices, replacing the electron acceptor TiO
2
with an insulating
alumina scaffold has played an important part in the increase
in open-circuit voltage.
[1]
This has been rationalized by the
presence of deep electron traps in the non-stoichiometric TiO
2
reducing the splitting of the quasi Fermi levels under illumina-
tion. The same mechanism is likely to affect ssDSSCs, but in
contrast to perovskite solar cells in which organometal trihalide
perovskites are a light absorbing charge transporter, ssDSSCs
rely on the metal oxide for charge transport, ruling out the use
of alumina or other insulating scaffolds.
[1]
In ssDSSCs, the dye is regenerated from its oxidised state
within a few hundred picoseconds, orders of magnitude faster
than in the iodide/triiodide-based liquid electrolyte cells, where
dye regeneration occurs on the microsecond time scale.
[6]
These extremely rapid regeneration dynamics should play
an important role in improved long-term stability of the dye
in the ssDSSC, since the dye is most likely to degrade in its
charged oxidized state.
[7]
However, to realize long-term stability
of DSSCs it is paramount to protect the organic components
of the device from oxidation by oxygen, moisture and other
oxidizing agents, by encapsulation in inert environment. We
have discovered a critical instability of mesoporous TiO
2
based
devices; when they are encapsulated in an inert atmosphere
and exposed to sunlight, a quick loss in device performance is
observed.
[8,9]
Encouragingly though, the cells recuperate to their
initial performance when the encapsulation is broken, exposing
them to air.
Here, we discuss in detail the nature of the titania surface
chemistry in the presence of oxygen and light, and its role in
Performance and Stability Enhancement of Dye-Sensitized
and Perovskite Solar Cells by Al Doping of TiO
2
Sandeep K. Pathak, A. Abate, P. Ruckdeschel, B. Roose, Karl C. Gödel, Yana Vaynzof,
Aditya Santhala, Shun-Ichiro Watanabe, Derek J. Hollman, Nakita Noel,
Alessandro Sepe, Ullrich Wiesner, Richard Friend, Henry J. Snaith,* and Ullrich Steiner*
Reversible photo-induced performance deterioration is observed in
mesoporous TiO
2
-containing devices in an inert environment. This phenom-
enon is correlated with the activation of deep trap sites due to astoichiom-
etry of the metal oxide. Interestingly, in air, these defects can be passivated
by oxygen adsorption. These results show that the doping of TiO
2
with
aluminium has a striking impact upon the density of sub-gap states and
enhances the conductivity by orders of magnitude. Dye-sensitized and per-
ovskite solar cells employing Al-doped TiO
2
have increased device efficiencies
and significantly enhanced operational device stability in inert atmospheres.
This performance and stability enhancement is attributed to the substitu-
tional incorporation of Al in the anatase lattice, “permanently” passivating
electronic trap sites in the bulk and at the surface of the TiO
2
.
DOI: 10.1002/adfm.201401658
Dr. S. K. Pathak, P. Ruckdeschel, B. Roose, K. C. Gödel,
Dr. Y. Vaynzof, A. Santhala, Dr. S.-I. Watanabe,
Dr. A. Sepe, Prof. R. H. Friend, Prof. U. Steiner
Cavendish Laboratory
Department of Physics
University of Cambridge
JJ Thomson Avenue CB3 0HE, UK
E-mail: h.snaith1@physics.ox.ac.uk
Dr. S. K. Pathak, Dr. A. Abate, D. J. Hollman,
N. Noel, Prof. H. J. Snaith
Clarendon Laboratory
Department of Physics
University of Oxford
Parks road, Oxford OX1 3PU, UK
E-mail: ullrich.steiner@unifr.ch
Prof. U. Wiesner
Material Science and Engineering
University of Cornell
214 Bard Hall, Ithaca, NY 14853-1501, USA
Prof. U. Steiner
Adolphe Merkle Institute
Chemin des Verdiers
CH-1700, Fribourg, Switzerland
1. Introduction
The commercial viability of a photovoltaic technology replacing
single-crystal silicon solar cells relies on three essential attrib-
utes: cost, performance and lifetime. While dye-sensitized
and more recently perovskite solar cell are highly promising
Adv. Funct. Mater. 2014,
DOI: 10.1002/adfm.201401658
www.afm-journal.de
www.MaterialsViews.com