Journal of Planar Chromatography 29 (2016) 3 1
1 Introduction
Carbaryl (1-naphthyl-N-methylcarbamate; Figure 1) belongs
to a family of chemicals that kill or control insects, known as
carbamates. These insecticides are widely used against a broad
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not be easily located, possibly because of biological impurities.
Figure 1
The chemical structure of carbaryl.
U.K. Kulkarni and K.V. Kulkarni, Directorate of Forensic Science Laboratories,
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E-mail:
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a mixture of sodium bromide and copper chloride for high-per-
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ane and ethyl acetate (9:1).
2 Experimental
2.1 Chemicals and Reagents
used throughout the analysis. Ten-percent ( v/v) sodium hydrox-
in 100 mL of distilled water.
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baryl (1 mg mL
) was prepared in ethanol. Similarly, all the
standards (profenofos, thiodan, cypermethrin, began, carbo-
for the extraction of carbaryl.
2.2 Extraction Procedure
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ple contains water, then diatomaceous earth is added to absorb
the water contents and get a solid and semisolid sample for ex-
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pieces along with diatomaceous earth and transferred into the
extraction cell. The extract was collected in a clean collection
and Detection of Carbaryl in Biological Materials
Ulka K. Kulkarni, Krishna V. Kulkarni, R.K. Pardeshi, and Dhananjay V. Mane*
Key Words:
Insecticide
High-performance thin-layer chromatography
Journal of Planar Chromatography 29 (2016) 3, 1–2 DOI: 10.1556/1006.2016.29.3.?
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