Advances in Materials Physics and Chemistry, 2012, 2, 239-248
http://dx.doi.org/10.4236/ampc.2012.24036 Published Online December 2012 (http://www.SciRP.org/journal/ampc)
In Silico Experiments of Carbon Dioxide Atmosphere and
Buffer Type Effects on the Biomimetic Coating with
Simulated Body Fluids
Gustavo M. Platt
1
, Ivan N. Bastos
1
, Mônica C. Andrade
1
, Glória D. A. Soares
2
1
State University of Rio de Janeiro, Nova Friburgo, Brazil
2
Federal University of Rio de Janeiro, Rio de Janeiro, Brazil
Email: gmplatt@iprj.uerj.br
Received September 29, 2012; revised October 29, 2012; accepted November 14, 2012
ABSTRACT
The formation of calcium phosphate phases is extremely important in a biomedical engineering context. These phos-
phates are used in many applications, such as grafts, drug-delivery processes and evaluation of the bioactivity of metal-
lic surfaces. Considering this scenario, it is useful to evaluate the thermodynamic conditions for the precipitation of
phosphates of biomedical interest, mainly hydroxyapatite. In this work, we investigate the effects of two important fac-
tors using a thermodynamic framework: 1) carbon dioxide partial pressure; and 2) buffer type (2-Amino-2-hydroxy-
methyl-propane-1,3-diol, known as TRIS and 2-[4-(2-hydroxyethyl)piperazin-1-yl] ethanesulfonic acid, also called
HEPES), on the driving force behind the precipitation of calcium phosphates in simulated body fluids. The in silico
results show that the pH value is governed by carbon dioxide content, as expected to occur in vivo. Moreover, the buff-
ers can deplete the free calcium available in solution and, consequently, can cause difficulties in the calcium phosphate
precipitation.
Keywords: Hydroxyapatite; Thermodynamic Modelling; Carbon Dioxide, HEPES and TRIS Buffers; In Silico
Experiments
1. Introduction
Hydrogen potential (pH) is a parameter of prime rele-
vance in aqueous liquid phases, either with in vivo or in
vitro situations. Therefore, species that are able to control
their pH values deserve special attention in these systems.
In the context of fluids that simulate those of body solu-
tions, two chemicals are very important: carbon dioxide
and buffers. In spite of this situation, few studies focus
on the thermodynamic aspects of these chemicals in the
precipitation of calcium phosphates.
Carbon dioxide partial pressure affects the pH of
aqueous solutions and can promote an increase/decrease
of carbonate/bicarbonate content in the liquid phase. In-
deed, its partial pressure plays a key role in in vivo pH
regulation.
The use of buffers is advisable in order to maintain the
pH of aqueous systems within narrow ranges and, thus,
several chemical reactions can take place under con-
trolled physico-chemical conditions. However, besides
protonation/deprotonation reactions of buffers, in some
cases, several complexation reactions can occur, mainly
with alkaline-earth ions. In these cases, the availability of
specific ions is diminished, influencing all chemical
equilibrium reactions, as well as the driving force to the
precipitation of phosphate phases when these ions take
part. In the specific case of calcium phosphates of bio-
medical interest, the quantity of free calcium ions in an
aqueous system is extremely important because this pa-
rameter affects the stoichiometry of solid phases (such as
hydroxyapatite). For example, using BISTRIS buffer, we
noted a drastic depletion of calcium ion concentrations in
simulated body fluids [1]. In the same context, Nakon
and Krishnamoorthy [2] showed that, among 20 buffers
known as “Good’s buffers”, three of them showed com-
plexation reactions with metal ions, interfering particu-
larly in protein analysis. In this paper, we analyze the
depletion of calcium ions in the presence of TRIS buffer,
comparing the results with HEPES buffer. Besides, the
determination of the carbon dioxide effects on calcium
phosphate precipitation was performed.
To evaluate the buffers and carbon dioxide in simu-
lated body fluids, we choose a thermodynamic analysis,
also known as in silico experiments, due to the scarcity
of works that use a similar theoretical approach.
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