ELSEVIER
Nuclear Instruments and Methods in Physics Research B 95 (1995) 102-106
B
Beam Interactions
with Materials & Atoms
PIXE and RBS analysis of sediments from E1-Kansera barrage on
Oued Beht river in Morocco
F. Benyaich a, L. Torrisi b,* M.Z. Benabdellah a, M. Derraz a
a Universit~ Moulay Isma~l, BP 4010 Beni M'Hamed, Mekn~s, Morocco
b Uniuersith di Messina, Ctr. Papardo, 31. 98166 S. Agata, Messina, Italy
Received 31 August 1994
Abstract
Elemental analyses of sediments from the barrage E1-Kansera on the river Oued Beht in Morocco, are reported. These
analyses were performed by means of proton induced X-ray emission (PIXE), and Rutherford backscattering spectroscopy
(RBS). The RBS analysis allowed the determination of the sediments matrix composition, which was used for the PIXE
analysis. The quantitative analyses of the PIXE spectra were performed by using the binary encounter approximation (BEA)
for the inner shell ionization cross section. Preliminary results are presented, and a comparison with literature data is
discussed.
1. Introduction 2. Experimental
Sediments in rivers estuaries, lakes and barrages have a
high capacity to concentrate and retain toxic trace ele-
ments. Heavy metals may be natural constituents of the
sediments, i.e. they come from the rocks and soils via their
geochemical mobility. They also can have anthropogenic
sources, in which case they are incorporated into the
sediments as artificial pollutants coming from urban, in-
dustrial or agricultural releases and wastes.
Developed and developing countries are paying an
increasing interest to environmental sciences due to the
evident impact industrialisation and urbanisation have on
the environment and the natural resources. In particular for
developing countries, given their geographical and climatic
situation, the disposability, the storage and the distribution
of good quality waters are matter of great concerns.
In the field of the environmental sciences, among the
many multi-elemental analysis techniques, ion beam analy-
sis (IBA) has demonstrated to be a powerful tool for
monitoring the elemental composition and trace elements
detection in soils, sediments, water and air particulates
[1-3]. In this paper we report on the elemental concentra-
tions of the sediments of the barrage E1-Kansera in Mor-
roco, measured by P1XE (proton induced X-ray emission)
and Rutherford backscattering spectroscopy (RBS).
* Corresponding author.
The analysed sediments samples were taken from the
basin storage of the barrage E1-Kansera in Morocco. This
barrage is located in the centre of Morocco near a small
urban agglomeration; Khemisset city in a farming region.
A schematic representation of the barrage and the incom-
ing rivers is drawn on Fig. 1. The barrage is filled by the
river Oued Beht and a small affluent Oued Khemisset
river. This barrage supplies Khemisset city and its region
with potable water and waters for agricultural uses. The
waste waters rejected from Khemisset city are drained by
the small affluent Oued Khemisset which feeds them back
into the main river Oued Beht. Oued Khemisset is a small
affluent and accounts for less than 10% of the total water
flux drained by Oued Beht.
The analysed sediments were taken from seven (7) sites
($1 to $7) in the basin storage as indicated in the insert of
Fig. 1. The sediments were collected from the superficial
layer of the sediments, i.e. the uppermost 3 cm. For each
site the sediments were collected from three points few
meter apart from each other and then mixed in order to
prepare homogeneous samples. The samples collection was
performed in the same day, in the order of the numerical
sequence of the inset of Fig. 1. The sediments were then
dried at 60°C and homogenised in an agate mortar. Thick
samples were pelletised into 1 cm diameter disks, their
mass was typically 250 mg. To avoid contamination of the
sediments during the preparation stage, both faces of the
compression die were covered with thin disks of polymer
(polytetrafluoroethylene).
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