Int J Thermophys (2011) 32:1732–1743
DOI 10.1007/s10765-011-0971-5
Investigations on Two Co–C Fixed-Point Cells Prepared
at INRIM and LNE-Cnam
M. Battuello · M. Florio · M. Sadli · F. Bourson
Received: 8 March 2010 / Accepted: 22 March 2011 / Published online: 8 April 2011
© Springer Science+Business Media, LLC 2011
Abstract INRIM and LNE-Cnam agreed to undertake a collaboration aimed to
verify, through the use of metal–carbon eutectic fixed-point cells, methods and facil-
ities used for defining the transition temperature of eutectic fixed points and manu-
facturing procedures of cells. To this purpose and as a first step of the cooperation, a
Co–C cell manufactured at LNE-Cnam was measured at INRIM and compared with
a local cell. The two cells were of different designs: the INRIM cell of 10 cm
3
inner
volume and the LNE-Cnam one of 3.9 cm
3
. The external dimensions of the two cells
were noticeably different, namely, 40 mm in length and 24 mm in diameter for the
LNE-Cnam cell 3Co4 and 110 mm in length and 42 mm in diameter for the INRIM
cell. Consequently, the investigation of the effect of temperature distributions in the
heating furnace was undertaken by implementing the cells inside single-zone and
three-zone furnaces. The transition temperature of the cell was determined at the two
institutes making use of different techniques: at INRIM radiation scales at 900 nm,
950 nm, and 1.6 μm were realized from In to Cu and then used to define T
90
(Co–C) by
extrapolation. At LNE-Cnam, a radiance comparator based on a grating monochro-
mator was used for the extrapolation from the Cu fixed point. This paper presents a
comparative description of the cells and the manufacturing methods and the results in
terms of equivalence between the two cells and melting temperatures determined at
INRIM and LNE-Cnam.
Keywords Cobalt–carbon · Fixed points · Metal–carbon eutectics ·
Radiation thermometry
M. Battuello (B ) · M. Florio
Thermodynamics Division, Istituto Nazionale di Ricerca Metrologica (INRIM), Turin, Italy
e-mail: m.battuello@inrim.it
M. Sadli · F. Bourson
Laboratoire Commun de Métrologie (LNE-Cnam), Saint Denis, France
123