Materials Science and Engineering B77 (2000) 210 – 212
Letter
Formation of glass microspheres with rotating electrical arc
Ioan Bica
West Uniersity of Timisoara, Bd. V. Paran no. 4, 1900 Timisoara, Romania
Received 5 April 2000; accepted 16 May 2000
Abstract
The paper presents the experimental device for obtaining glass microspheres in rotating electrical arc. With this device, for arc
power values of 5 ×10
3
W and for frequency of =850 s
-1
, the glass powder with arbitrary shaped particles was transformed
in microsphere with diameters between 2 and 24 m and the wall thickness between 0.4 and 1.6 m. The particles in the powder
were up to 30 m in diameters, have a flow rate of 2 g·min
-1
and were transported in argon (5 Nl min
-1
). The mean diameter
is d =5.62 m. © 2000 Elsevier Science S.A. All rights reserved.
Keywords: Rotating electric arc; Glass powder; Microspheres
www.elsevier.com/locate/mseb
1. Introduction
Glass microspheres are made of sputtered materials
(known in general). The raw material used is specific to
commercial glass or to special behaviour glass. By
melting with flame or/and vaporization in plasma, in
certain conditions, microspheres of glass are obtained.
They are used for obtaining reflecting paints, reflect-
ing layers and for dielectric materials with a certain
dielectric permittivity [1]. Recently, glass microspheres
have been in magneto-fluidic composites applied in
selective absorbants of mechanical shocks [2,3] and
earthquake waves [3,4] and in sensors, respectively [5].
Inner and outer diameters of microsphere are sup-
posed to have pre-established values. Chemical compo-
sition and surface conditions should be such that the
elasticity coefficients have values suitable for applica-
tions and small meeting energy respectively.
Consequently, flexible methods for obtaining glass
microspheres for several applications are of interest.
Such a method is presented below.
2. Experimental device
The experimental device, designed for obtaining the
microspheres in rotating electrical arc plasma is pre-
sented in Fig. 1. The electrical arc between electrodes 1
and 2 is supplied by the current source 3, at a value I of
electrical discharge current. Coils 4 and 5 produce a
magnetic field so that the induction B is perpendicular
to the density of electrical discharge current vector j.
The interaction between the magnetic field and the
current results in the effect of Lorentz force F =j ×B,
i.e. the rotation of the electric arc. The frequency is
measured by the device 6. By means of the device 7,
under the gas pressure, the glass particles, with pre-es-
tablished flow rate, are carried in the thermal ionized
gas.
3. Results and discussions
Particles obtained from glass mechanical processing
have the shape and dimensions as shown in Fig. 2.
After sieving, samples of particles with dimensions up
to 30 m were obtained. Parameters of the rotating
electrical arc are those used for making spherical parti-
cles made up of chamote rod [6] i.e.:
electrical discharge current intensity, I =100 A
d.c.
;
arc electrical voltage, U =50 V
d.c.
;
total magnetic field induction, B =26 mT;
rotating frequency of the electrical arc, =850 s
-1
;
plasmagen gas flow rate (Ar), D =7.5 Nl min
-1
;
carrier gas flow rate (Ar), D
c
=5 Nl min
-1
.
0921-5107/00/$ - see front matter © 2000 Elsevier Science S.A. All rights reserved.
PII:S0921-5107(00)00483-9