Effect of Talc on the Properties of Polypropylene/Ethylene/
Propylene/Diene Terpolymer Blends
Mustafa O
¨
ksu ¨ z,
1
Mehmet Eroglu,
2
Hu ¨ seyin Yıldırım
3
1
Technical Education Faculty, Marmara University, 34722 Goztepe, Istanbul, Turkey
2
Department of Metallurgical and Materials Engineering, Engineering Faculty, Fırat University, 23119, Elazig, Turkey
3
Department of Chemistry, Yıldız Technical University, 34210 Esenler, I
˙
stanbul, Turkey
Received 15 March 2005; accepted 5 October 2005
DOI 10.1002/app.23699
Published online in Wiley InterScience (www.interscience.wiley.com).
ABSTRACT: In the present study, the effect of talc content
on the mechanical, thermal, and microstructural properties
of the isotactic polypropylene (i-PP) and elastomeric ethyl-
ene/propylene/diene terpolymer (EPDM) blends were in-
vestigated. In the experimental study, five different talc
concentrations, 3, 6, 9, 12, and 15 wt %, were added to
i-PP/EPDM (88/12) blends to produce ternary composites.
The mechanical properties such as yield and tensile
strengths, elongation at break, elasticity modulus, izod im-
pact strength for notch tip radius of 1 mm, and hardness
with and without heat treatments and thermal properties,
such as melt flow index (MFI), of the ternary composites
have been investigated. The annealing heat treatment was
carried out at 100°C for holding time of 75 h. From the
tensile test results, an increased trend for the yield and
tensile strengths and elasticity modulus was seen for lower
talc contents, while elongation at break showed a sharp
decrease with the addition of talc. In the case of MFI, talc
addition decreased the MFI of i-PP/EPDM blends. It was
concluded that, taking into consideration, mechanical prop-
erties and annealing heat treatment, heat treatment has
much more effect on higher yield and tensile strengths,
elongation at break, elasticity modulus, impact strength, and
hardness. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101:
3033–3039, 2006
Key words: poly(propylene) (PP); talc; EPDM; mechanical
properties; heat treatment
INTRODUCTION
Particulate filled polymers have been a subject of in-
creasing interest in both industry and research.
Polypropylene (PP) has a good processability allowing
to accept numerous types of natural and synthetic
fillers. The incorporation of fillers such as kaolin, mica,
talc, and calcium carbonate into thermoplastics is a
common practice to reduce production costs and to
improve the properties such as strength, stiffness,
hardness, flexural modules, dimensional stability,
crystallinity, electrical, and thermal conductivity.
However, high filler additions may adversely affect
the processability, ductility, and strength of compos-
ites. The properties of the composites strongly depend
on the interfacial adhesion between filler and matrix.
In case the adhesion is strong at the interface of filler
and matrix, the mechanical properties may in-
crease.
1–10
Although PP has been used widely in a variety of
application because of its advantages, such as low
density, low cost, high softening points, and easy pro-
cessing, it has low impact strength especially at low
temperatures and this limits its application as an engi-
neering thermoplastic. To improve the impact strength,
various elastomers, such as ethylene–propylene– copol-
ymer, ethylene–propylene– diene terpolymer (EPDM),
and ethylene-vinyl acetate, were blended with PP.
Among these elastomers, EPDM is considered as one
of the most effective impact modifiers for PP. Al-
though toughness strength is improved by blending
elastomer, this results in deteriorating tensile strength
and modulus. Therefore, numerous studies have been
performed to improve the toughness, stiffness, and
strength balance. Therefore, PP has been modified by
different fillers and elastomers. The mechanical prop-
erties of such ternary composites strongly depend on
their composition and characteristic of the compo-
nents and the phase morphology, and in particular
relative dispersion of additive components. In the ter-
nary composites containing both elastomer and rigid
fillers, two different types in phase structure may
occur, where elastomer and filler particles are dis-
persed separately on the PP matrix or the rubber
encapsulates fillers particles, resulting in a low mod-
ulus interlayer between matrix and filler.
11–21
In the literature, there are some published studies
relating to PP/elastomer/filler ternary compos-
ites.
11–20
However, the effect of talc with heat treat-
Correspondence to: M. O
¨
ksu ¨ z (moksuz@marmara.edu.tr).
Contract grant sponsor: Commission of Scientific Re-
search Projects of the University of Marmara (FEN 105/
020603).
Journal of Applied Polymer Science, Vol. 101, 3033–3039 (2006)
© 2006 Wiley Periodicals, Inc.