Journal of Crystal Growth 198/199 (1999) 844—849 Microstructure of Ni—Ni Si eutectic alloy produced by directional solidification Rubens Caram*, Srdjan Milenkovic State University of Campinas, C.P. 6122, 13083-970, Campinas-SP Brazil Abstract The microstructures and solidification behaviour of Ni—Ni Si eutectic composite have been studied systematically. Samples were processed in a Bridgman type solidification furnace using induction heating with growth rates ranging from 6.5 to 20.0 mm/h. During directional solidification, Ni—Ni Si eutectic is characterised by cell and dendrite—free and well-aligned lamellar structure on a micron scale. The scaling laws of the variation in lamellar spacing () with growth rate (») are quantitatively developed. Despite the presence of an intermetallic phase, highly regular structure was obtained and no lamellar spacing selection problem was observed. 1999 Elsevier Science B.V. All rights reserved. Keywords: Directional solidification; Eutectic growth; Lamellar microstructure 1. Introduction The galloping industrial and technological devel- opment has induced an extensive search for the advanced materials for high-temperature applica- tions. Among a wide variety of materials, com- posite materials seem to have the greatest potential to meet ever increasing requirements [1]. A subset of this class of materials is natural or in situ composites. They can be produced, besides the con- ventional methods, by directional solidification of eutectic alloys. The advantages of this technique * Corresponding author. Tel.: #55 19 788 79 66; fax: #55 19 2893722; e-mail: caram@fem.unicamp.br. over the conventional one are manifest: it involves the extension of a well established technology, allows components to be produced from the melt in a single stage process, and leads to a composite of phases that are thermodynamically stable, chemic- ally compatible, well aligned and finely dispersed. Thus, directional solidification has received con- siderable attention in the past few decades. In the 1960s, directional solidification was developed to process eutectic alloys [2—5]. Research was initially focused on materials for high temperature struc- tural applications, but it was soon broadened to non-structural materials for electronic, magnetic, and optical applications [6]. The vast majority of technically important eutec- tic alloys are composed of two phases. Directional solidification of binary or pseudo-binary eutectics, 0022-0248/99/$ — see front matter 1999 Elsevier Science B.V. All rights reserved. PII: S 0 0 2 2 - 0 2 4 8 ( 9 8 ) 0 1 1 4 3 - 9