HYBRID FABRICATION OF MICROFLUIDIC CHIPS BASED ON COC,
SILICON AND TMMF DRY RESIST
Kiril Kalkandjiev
1
, Roland Zengerle
1
and Peter Koltay
1,2
1
University of Freiburg - IMTEK, Germany
2
BioFluidiX, Freiburg, Germany
ABSTRACT
We describe the hybrid fabrication of silicon-plastic
microfluidic chips based on machining of Cyclic
Olefin Copolymer (COC), standard silicon process-
ing and TMMF lithography. The combination of
different processes enables an individual material
selection leading to significant reduction of the
manufacturing costs. We demonstrate the potential
of the hybrid technology by manufacturing and
testing a 24-channel TopSpot dispenser [1] which
consists of an intermediate silicon layer, a COC
interface and a TMMF sealing lid. Characterization
studies show that TMMF lamination is ideally
suited for the sealing of silicon microchannels
showing numerous advantages over adhesive-based
approaches, thermal and anodic bonding.
INTRODUCTION
In contrast to sensor devices manufactured in
batches of thousands, BioMEMS devices are often
requested in smaller numbers, which makes low-
cost fabrication challenging. While silicon proc-
esses go for higher densities and sub-micron struc-
tures, the size of a typical microfluidic device is
given by the relatively large interface that requires
thicker materials for operation with laboratory-scale
equipments [2]. As a result, polymer techniques
have been adapted for the requirements of
BioMEMS. The main advantages of polymers –
lower cost compared to silicon and glass, wide
range of available materials and suitability for pro-
totyping and high-volume production, have been
frequently pointed out [3-5]. On the other hand,
silicon components have the advantage of higher
accuracy as a consequence of the established
MEMS processes. Silicon is the material of choice
when components with high-aspect ratio, sharply
defined edges or high mechanical stiffness are re-
quired. It is furthermore advantageous when it
comes to the integration of sensing or actuating
elements [6].
Silicon micromachining is often combined with
silicon-Pyrex anodic bonding to provide the chip
with the necessary peripheral components. The
machining of Pyrex, however, together with the
anodic bonding and dicing of the stacked assembly
is a time-consuming process that accounts for a
very significant part of the manufacturing costs. At
the same time, the properties of the Pyrex compo-
nents and the high quality of the anodic bond are
not necessarily required for a typical lab-on-a-chip.
Thus, silicon-plastic hybrid integration approaches
should be considered as an open alternative for cost
saving. A major aspect of the hybrid integration is
the precise alignment and liquid-tight bonding of
components possessing different chemical nature.
Usually, bonding of dissimilar materials is based on
the use of adhesives. In microfluidics, however,
direct bonding is more popular [7] but it is mostly
restricted to materials of the same type.
Few methods for direct silicon-plastic bonding such
as localized heating with resistive heaters [8,9],
plasma-assisted silicon-PDMS bonding [10], me-
chanical interlocking [11] or bonding of polymer to
a black-silicon surface [12] have been reported to
be suitable for the fabrication of hybrid liquid-tight
assemblies.
In this paper, we describe an alternative fabrication
technique using TMMF dry resist as a sealing lid
for silicon microchannels and an adhesive tape (3M
9965) for bonding of the silicon core to a COC
interface. Finally, we show the application of this
technique to the manufacturing of 24-channel Top-
Spot printheads used for the formation of microar-
rays [1].
FABRICATION
The printhead contains 24 reservoirs which can be
filled with different samples using standard labora-
tory equipment. Each reservoir is connected to a
corresponding nozzle via a capillary microchannel.
The nozzles are arranged in a 6x4 grid with a pitch
of 500 µm. A one-to-one format conversion from
the 4.5 mm pitched reservoirs to the microarray
format is provided by the microchannels. A piezo-
driven piston generates a pressure pulse by com-
pressing an air chamber which causes the parallel
ejection of a single droplet out of each nozzle
(Fig. 1).
Figure 1: A schematic cross-section and operation
principle of the hybrid TopSpot printheads.
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