shown in Fig. 2a, radioactivities released from the con-
trol vesicles were very low and essentially constant
within the experimental period indicating that the
leakage of
45
Ca
2+
incorporated into the sealed vesicles
is, if any, negligible even in the presence of Brij 58. In
contrast, appreciable amounts of
45
Ca
2+
were dis-
charged from the vesicles when physiological concen-
tration of cyclic AMP (3) or valinomycin was added to
the suspension of the vesicles (Fig. 2a). Approximately
31 and 33% of
45
Ca
2+
in the sealed vesicles were re-
leased by the treatment with cyclic AMP and valino-
mycin, respectively, suggesting that the activities of
the cyclic nucleotide-dependent and voltage-dependent
Ca
2+
channels were not lost by the treatment with the
detergent. In order to compare the activities of Ca
2+
channels in the absence and presence of Brij 58,
45
Ca
2+
-
loaded vesicles were similarly prepared and treated
with cyclic AMP and valinomycin in the absence of the
detergent (Fig. 2b). Although a fluctuation of the ra-
dioactivities was observed in the detergent-free vesi-
cles, 39 and 34%
45
Ca
2+
were released by the treatment
with cyclic AMP and valinomycin, respectively. Even if
considering the unstable background radioactivities,
these figures appeared to be similar to those obtained
in the Brij 58-treated vesicles (Fig. 2a). Since
45
Ca
2+
is
loaded into and discharged from solely inside-out-ori-
ented vesicles under the detergent-free condition, it is
reasonable to conclude that activities of plasma mem-
brane-located Ca
2+
channels stimulated by cyclic AMP
or K
+
flux are not reduced even in the presence of 0.2%
Brij 58.
In conclusion, determination of
45
Ca
2+
discharged
from the ion-loaded sealed vesicles of plant plasma
membrane reoriented with Brij 58 is a convenient
method to assess Ca
2+
influx triggered by the changes
in inter- and intracellular conditions of higher plants.
Environments inside and outside of intact plant cells
can be readily mimicked appropriately, and the signal/
noise ratio (the ratio of discharged
45
Ca
2+
to “back-
ground” radioactivities) has been greatly increased by
the reorientation of the vesicles without inactivation of
the channel proteins.
Acknowledgment. This work was supported in part by a Grant-
in-Aid from the Ministry of Education, Science and Culture, Japan.
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Acad. Sci. USA 97, 9323– 9328.
Calsequestrin Blot Overlay of Two-Dimensional
Electrophoretically Separated Microsomal
Proteins from Skeletal Muscle
Louise Glover, Gabriele Froemming, and
Kay Ohlendieck
1
Department of Pharmacology, Conway Institute of
Biomolecular and Biomedical Research, University College
Dublin, Belfield, Dublin 4, Ireland
Received June 25, 2001; published online November 10, 2001
Calsequestrin represents a medium-affinity, high-
capacity Ca
2+
-binding protein of the sarcoplasmic re-
ticulum (1, 2) and plays a central role in the regulation
of the excitation– contraction–relaxation cycle in skel-
etal muscle (3, 4). Although the physiological and bio-
chemical characterization of this terminal cisternae
protein (5–7), as well as electron microscopical studies
(8, 9), strongly suggest that calsequestrin forms large
protein aggregates, no direct biochemical evidence ex-
ists demonstrating protein–protein interactions within
triadic Ca
2+
-binding units. In determining protein
linkage biochemically, one-dimensional (1D)
2
gel elec-
trophoretic separation and blotting methodology em-
ploying purified proteins have been established as
effective tools. However, interactions between immobi-
lized calsequestrin and purified calsequestrin failed in
a previous blot overlay attempt (10). Only low molecu-
lar mass calsequestrin-binding proteins such as junc-
tin were identified (10). Thus, to demonstrate direct
coupling between calsequestrin monomers of apparent
63 kDa, we advanced the overlay blotting technique in
the following manner: (a) instead of 1D blots, nitrocel-
1
To whom correspondence and reprint requests should be ad-
dressed. E-mail: kay.ohlendieck@ucd.ie.
2
Abbreviations used: 1D, one-dimensional; 2D, two-dimensional;
CSQ, calsequestrin.
268 NOTES & TIPS
Analytical Biochemistry 299, 268 –271 (2001)
doi:10.1006/abio.2001.5424
0003-2697/01 $35.00
© 2001 Elsevier Science
All rights reserved.