Pergamon
Tetrahedron: Asymmetry, Vol. 7, No. 5, pp. 1419-1430,1996
Copyright© 1996ElsevierScience Ltd
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Synthesis of Phosphinoferrocenyloxazolines. New Ligands for
Asymmetric Catalysis
Christopher J. Richards* and Andrew W. Mulvaney
Departmentof Chemistry, University of Wales, Cardiff, PO Box 912, Cardiff, CF1 3TB, UK.
Abstract: Condensation of [3-hydroxy alcohols with ferrocenyl chloride gave the
corresponding amides which were dehydrated to give ferrocenyl oxazolines in good overall
yield. Subsequent lithiation with n-BuLl in the presence of TMEDA and addition of PPh2C1
led to the isolation of (S)-(s)-ipr-phosferrox and (S)-(S)-Me-phosferrox ligands 1 and 2. Their
corresponding diastereoisomers, (S)-(R)JPr-phosferrox and (S)-(R)-Me-phosferrox 3 and 4
were obtained via the intermediacy of removable trimethylsilyl blocking groups. The CD
spectra of 1 - 4 and their parent ferrocenyl oxazolines 9 and 10 were obtained.
Copyright © 1996 Elsevier Science Ltd
Introduction
Ferrocene-derived ligands utilise the planar chirality that results when the ferrocene nucleus contains
two different substituents attached to a cyclopentadienyl ring. 1 Of the examples known, most are derived from
N,N-dimethyl-1-ferrocenylethylamine as this can be obtained enantiomerically pure by classical resolution2 or
asymmetric synthesis) In contrast, oxazoline ligands exploit the tetrahedral stereocentres inherent in the
amino acids from which they are derived. On coordination, their 4-substituent lies proximal to the metal
thereby influencing the stereoselectivity of catalysed reactions. 4 In particular, phosphinoaryloxazolines
containing electronically unsymmetrical nitrogen and phosphorous coordinating groups, have proved to be
very successful ligands for asymmetric allylic substitution reactions. 5 Thus attaching oxazolines to an
appropriate ferrocene nucleus has the potential benefits of cooperatively combining the tetrahedral chirality
inherent in the oxazoline with the planar chirality of disubstituted ferrocenes. 6
O
?3 Ph2 Ph2
N Me Me
N ...... (
Fe~" PPh2 IMe Fe PPh2 Fe Me Fe
1 2 3 4
(S)- (s)-ipr-phos ferrox (S)-(S)-Me-phos ferrox (S)-(R)-ipr-phosferrox (S)-(R)-Me-phosferrox
Phosferrox ligands
1419