Hydrometallurgy, 27 (1991) 169-177 169
Elsevier Science Publishers B.V., Amsterdam
Liquid-liquid extraction of yttrium (III) with
mixtures of organophosphorus extractants:
theoretical analysis of extraction behaviour
P.B. Santhi, M.L.P. Reddy*, T.R. Ramamohan and A.D. Damodaran
Regional Research Laboratory (CSIR), Trivandrum-695019, India
(Received September 10, 1990; revised version accepted February 23, 1991 )
ABSTRACT
Santhi, P.B., Reddy, M.L.P., Ramamohan, T.R. and Damodaran, A.D., 199 h Liquid-liquid extrac-
tion of yttrium (Ill) with mixtures oforganophosphorus extractants: theoretical analysis of exlrac-
tion behaviour. Hydrometallurgy, 27:169-177.
The extraction of yttrium (III) from chloride solutions with mixtures of 2-ethylhexylphosphonic
acid mono-2-ethylhexyl ester (EHEHPA) and di-2-ethylhexylphosphoric acid (DEHPA) or tri-n-octyl
phosphine oxide (TOPO) in kerosene has been studied systematically over a wide range of condi-
tions. A relatively small synergistic enhancement has been observed with mixtures of acidic
organophosphorus extractants (EHEHPA+ DEHPA). On the other hand, antagonistic effects have
been observed with mixtures of acidic and neutral organophosphorus compounds
(EHEHPA+TOPO). These extraction data have been analysed theoretically taking into account
complexation of the metal in the aqueous phase by inorganic ligands and plausible complexation in
the organic phase.
INTRODUCTION
The synergistic extraction of rare earths by mixtures of a chelating agent
and a neutral donor has been studied extensively by several authors and these
data are covered in excellent reviews on synergistic extraction [ 1-3 ]. Tachi-
mori and Nakumara [4 ] have studied the synergistic extraction of Nd (III)
with mixtures of mono (2-ethylhexyl)phosphoric acid (MEHPA) and di-2-
ethylhexylphosphoric acid (DEHPA). Nemoto and co-workers [ 5 ] have also
successfully applied a mixed solvent (DEHPA + MEHPA) to the extraction
of lanthanides. Sato and Ban [6 ] have studied the effect of the addition of
TOPO on the extraction of rare earths from hydrochloric acid solutions by
DEHPA and EHEHPA. However, no detailed studies relevant to the syner-
gistic effects on the extraction of yttrium (III) with mixtures of 2-ethyl-
*To whom correspondence should be addressed.
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