future science group 61 ISSN 1759-7269 10.4155/BFS.11.150 © 2012 Future Science Ltd
In 1950 Reese et al. proposed a mechanism for cel-
lulose hydrolysis, which involved two general com-
ponents, C
1
and C
x
, acting in sequence [1] . According
to the model, the C
1
component first disrupted and
swelled the crystalline cellulose, possibly releasing
soluble oligosaccharides into solution. The C
x
compo-
nent, which was shown to have endoglucanase activity,
was then able to effectively hydrolyze the previously
inaccessible substrate along with the soluble oligo-
saccharides. Furthermore, the activity of the mixture
was found to be higher than the activity of each com-
ponent acting alone, indicating that the components
were acting synergistically. In the following years, a
number of groups began to identify and characterize
the specific enzymes present in these components. It
became clear that in addition to the endoglucanase
activity demonstrated originally for the C
x
component,
exoglucanase activity was also present in the filtrates
of cellulolytic organisms and that the combination of
exo- and endo- activities resulted in the synergistic
hydrolysis of cellulose [2–5] . In 1979, Wood and McCrae
summarized the findings and proposed what became
the classical endo–exo model of enzymatic cellulose
hydrolysis [6] . According to this model, endocellulases
attack the bulk cellulose, creating new chain ends that
are susceptible to exocellulase digestion. Exocellulases
in turn create more substrate for endocellulases by
disrupting the crystalline substrate and/or by expos-
ing previously inaccessible less ordered substrate that
is susceptible to attack by endocellulases. With time it
became evident that some exocellulases are also able
to act synergistically with each other [7–10] , giving rise
to the suggestion that there are two classes of exocel-
lulases that preferentially attack either the reducing or
the nonreducing end of the cellulose chain. This was
definitively demonstrated by Barr et al. in 1996 using
14
O- and
14
C-labeled cellooligosaccharides [11] .
It seems likely that synergism occurs only when
two cellulases attack different regions of the cellulose
microfibril and that each enzyme creates new sites of
attack for other enzymes in the mixture. However, this
is an oversimplification of a complex process that is still
not completely understood. There is no current evi-
dence that synergism requires interactions between the
synergizing cellulases, since cellulases from unrelated
organisms, which would not have sites for binding to
each other, often show cross synergism. However, it is
not known if synergizing cellulases interact when they
are bound to cellulose, and there could be interactions
caused by two enzymes binding to a specific site on the
cellulose. b-glucosidases, which cleave cellobiose and,
to lesser extent, other oligosaccharides [12] to glucose,
Biofuels (2012) 3(1), 61–70
Synergistic interactions in cellulose hydrolysis
Maxim Kostylev & David Wilson*
Cellulases acting on crystalline cellulose in synergistic mixtures have higher combined activities than the
sum of their individual activities. The mechanisms by which diferent types of cellulases enhance each
other’s activities are complex and not completely understood, and the published data is often inconsistent.
We discuss the role of the substrate and experimental factors in synergism experiments and consider the
various modes of synergism that have been proposed. New oxidoreductase enzymes that participate in
novel synergistic reactions are also discussed. Finally, we propose a general encompassing synergism
model, based on the observations described in the review.
REVIEW
Department of Molecular Biology and Genetics, Cornell University, 458 Biotechnology Building, Ithaca, NY 14853, USA
*Author for correspondence: Tel.: +1 607 255 5706; Fax: +1 607 255 5706; E-mail: dbw3@cornell.edu