International Geology Review, Vol. 50, 2008, p. 848–862. DOI: 10.2747/0020-6814.50.9.848
Copyright © 2008 by Bellwether Publishing, Ltd. All rights reserved.
0020-6814/08/1018/848-15 $25.00 848
Fluid Inclusion and Stable Isotope Characteristics of
the Arapuçandere Pb-Zn-Cu Deposits, Northwest Turkey
GÜLCAN BOZKAYA,
1
AHMET GÖKÇE
Cumhuriyet University, Department of Geological Engineering, 58140 Sivas, Turkey
AND NATHALIE V. GRASSINEAU
Royal Holloway University of London, Department of Geology, Egham, United Kingdom
Abstract
The Arapuçandere Pb-Zn-Cu ores are typical examples of vein-type lead-zinc deposits in the
Biga Peninsula. Permian–Triassic metamorphic, Triassic metaclastic and metabasic rocks,
Oligocene–Miocene granitoids, Miocene volcanic rocks, and Quaternary terrestrial sediments crop
out in the study area. The veins occupy fault zones in Triassic metasandstone (meta-arkose and
subarkose) and metadiabase, and contain galena, sphalerite, chalcopyrite, pyrite, marcasite, covel-
lite and specular hematite as ore minerals, with quartz, calcite, and barite as gangue minerals. Based
on macro- and micro-petrographic investigations, sulfide minerals formed in the earliest stage of
mineralization, and were followed by quartz and calcite crystallization. Fluid inclusion studies
showed that salinity (avg. 18.3%) was low, but that temperature was relatively high (avg. 301.4°C)
during stages of sulfide precipitation. In contrast, the salinity (avg. 27.1% NaCl equiv.) increased
and the temperature (avg. 240.2°C) decreased during crystallization of the quartz. Finally, the salin-
ity and temperature of the fluid gradually declined through the later episode of mineralization when
the primary and secondary inclusions in calcite formed. Isotopic compositions of the aqueous fluid
(δ
18
O = –7.5 to –1.7‰, and δD = –90 to –55‰) indicate the presence of meteoric water modified
slightly by fluid-rock interaction.
A geologic and genetic relation between ore veins and Oligo-Miocene granitoids and Miocene
volcanic rocks appears to be lacking. The ore and host-rock relations suggest only a post-Triassic
age for the mineralization. Pb-isotope model ages suggest a pre-Eocene age for the mineralization,
which predated Oligo-Miocene granitoid emplacement and Miocene volcanic activity. We conclude
that the Pb-Zn-Cu veins in the study area formed by deeply circulating meteoric water. The metals
and sulfur were leached from the surrounding pre-Eocene units and deposited along fault zones.
Introduction
PB-ZN-CU deposits are widespread in the Biga Pen-
insula. Some of the deposits hosted by metamorphic
rocks are pre-metamorphic in occurrence, and thus
bear the effects of regional recrystallization. How-
ever, most are vein-type deposits hosted by various
rock types, including Paleozoic metamorphic rocks,
Permo-Triassic clastic and calcareous rocks, and
Tertiary volcanic rocks.
In recent years, the first two authors of the pres-
ent paper began carrying out detailed geological,
ore-petrographic, fluid inclusion, and stable- and
Pb-isotopic studies on various deposits of the Biga
Peninsula in order to identify similarities and differ-
ences among deposits in different units of varying
lithology and age—e.g., Koru (Bozkaya, 2001;
Bozkaya and Gökce, 2001, 2002, 2006), Balcilar
(Bozkaya, 2003, Bozkaya and Gökce, 2007),
Kumarlar (Bozkaya and Çelik, 2007). These previ-
ous studies showed that the S-isotopic compositions
and fluid-related characteristics of these deposits
differ in accordance with age and host lithology, and
that the genesis of the various deposit types needs to
be studied separately.
The present study focuses on the microthermo-
metric and isotopic characteristics of the fluids
trapped in fluid inclusions within quartz in order to
elucidate the origin of the mineralizing hydrother-
mal solutions in the Arapuçandere Pb-Zn-Cu depos-
its, and the genesis of this and similar deposits in
the region.
The Arapuçandere Pb-Zn-Cu deposits, located
in the northwestern part of the Yenice district of
1
Corresponding author; email: gbozkaya@cumhuriyet.edu.tr