IJSRSET1626122 | Received : 10 Dec. 2016 | Accepted : 20 Dec. 2016 | November-December-2016 [(2) 6: 512-514 ]
© 2016 IJSRSET | Volume 2 | Issue 6 | Print ISSN: 2395-1990 | Online ISSN : 2394-4099
Themed Section: Science and Technology
512
FTIR Spectroscopic Studies on the Complex of Dl-Methionine
with Trichloreacetic ACID
R. Poornashri Mathangi
*
, A. Sajitha Banu
Department of Physics, PSNA College of Engineering and Technology, Dindigul, Tamil Nadu India
ABSTRACT
The main objective of this present work is to grow a single crystal of complex DL-METHIONINE with
TRICHLOREACETIC ACID and to investigate with FTIR spectroscopy.
Keywords: Solution growth, FTIR, Vibrational Spectra.
I. INTRODUCTION
Crystal:
A crystal is a solid in which the constituent atoms,
molecules or ions are packed in a regular order with
repeating pattern extending in all three spatial
dimensions. The word crystal originates from the
Greek word “ Krystallos” meaning “ clear ice”, as it
was thought to be especially solid form of water. Most
metals encountered in everyday life are poly crystals.
Crystals are often symmetrically inter grown to form
crystal twins [3]. Crystal refers to solid objects that
exhibit well-defined and often pleasing geometric
shapes. Many types of crystals are found in nature.
Snow flakes, diamonds and common salts are common
examples of crystals.
Crystallography
To acquire fundamental data and to explore the
properties of any solid state device, good quality
single crystal is essential. Hence crystal growth has
become the most vital and fundamental part of
material science, engineering, physical science,
biology etc. Single crystals of SiC, Ga As, InP are in
great demand. Crystallography is the scientific study
of crystals and crystal formation. It is often employed
by materials scientists. The understanding of crystal
structures is an important prerequisite for
understanding crystallographic defects. A number of
physical properties are linked to crystallography.
Crystal Structure
The process of forming a crystalline structure is often
referred to as crystallization. While the cooling
process generally results in generation of crystalline
material, under certain conditions, the fluid may be
frozen in a non-crystalline state. Crystalline structure
occurs in all classes of materials, with all types of
chemical bonds. Almost all metal exists in a
polycrystalline state; amorphous or single crystal
metals must be produced synthetically, often with
great difficulty. In a single crystal, the crystal lattice of
the entire sample is continuous and unbroken to the
edges of the sample, without any grain boundaries.
But a polycrystalline sample is made up of number of
small crystals known as crystallites.
Crystal Growth Techniques
The main categories of crystal growth techniques are:
1. Solid growth: It involves solid – solid phase
transitions.
2. Melt growth: It involves liquid – solid phase
transitions.
3. Vapour growth: It involves vapour – solid phase
transitions.