ISSN 0036-0244, Russian Journal of Physical Chemistry A, 2012, Vol. 86, No. 8, pp. 1204–1207. © Pleiades Publishing, Ltd., 2012.
1204
1
INTRODUCTION
Ultrasonic velocity affects the physical properties
of the medium and hence one can furnish information
about the liquid and liquid mixtures. In recent years,
ultrasonic velocity is gaining importance in under-
standing the nature of solute-solvent interactions [1].
Knowledge of thermodynamic and acoustical proper-
ties is of great significant in studying the physical
behavior and molecular interactions in a variety of liq-
uid mixtures of pure [2, 3], liquid mixtures [4–6] and
electrolytic solutions [7–10]. A survey of literature
shows that scanty work has been done on binary mix-
tures of phenol with some organic liquids [4, 5]. The
present work reports evaluation of some acoustical
parameters of ternary mixtures of toluene + chloro-
form + cyclohexane at 303.15, 308.15, and 313.15 K.
The adiabatic compressibility, intermolecular free
length, free volume, internal pressure, acoustical
impedance, Rao’s constant and Wada’s constant of
mixtures at various temperatures haven been studied
in the present paper. Such data are expected to high-
light the role of solute and solvents in the solutions and
its influence on temperature.
EXPERIMENTAL
The ultrasonic velocity in the liquid mixtures have
been measured using an ultrasonic interferometer
1
The article is published in the original.
(Mittal type-82, New Delhi, India) working at 2 MHz
frequency with accuracy ±0.1 m s
–1
. The interferometer
is a fixed frequency variable path type. Ultrasound of
constant frequency is generated at the bottom of the
cylindrical sample cell using quartz crystal and is sent
into the medium under study. The propagated waves
after getting reflected at the reflector surface held at the
top of the cell, again travels back through the same
medium. These two waves form stationary wave pattern
and hence nodes and antinodes are formed in the
medium. A fine micrometer screw is provided in the set
up that allows for finer movements of the reflector plate
in the medium. Thus moving the reflector plate for a
fixed number of antinode (or node) positions, the dis-
tance moved for a known number of waves can be
known. Use of frequency with these data will yield the
sound velocity in the medium. The density and viscosity
are measured using a pycnometer and an Oswald’s vis-
cometer of accuracy of ±0.1 kg m
–3
and 0.001 m N cm
–2
respectively. The samples are Anala2R grade of purity
99.5% and used directly with out purification. The val-
ues of density, viscosity and velocity of pure samples
are agreed well with the standard reference values. In
all systems, the mole fraction of the second compo-
nent, chloroform (x
2
= 0.2) was kept constant, while
the mole fraction of the remaining (x
1
and x
3
) were
varied from 0.1 to 0.8 as to have the different compo-
sitions [11].
Acoustical Parameters of Toluene + Chloroform + Cyclohexane
Mixtures at 303.15, 308.15, and 313.15 K
1
V. Vanathi
a
, S. Mullainathan
a
, and S. Nithiyanantham
b
a
Department of Physics, AVC College of Engineering, Mayiladuthurai, Tamil nadu, India 609306
b
School of Physical Sciences and Nanotechnology, (Biophysics/Ultrasonics Division), SRM University,
Kattankulathur, Tamil nadu, India 603203
E-mail: s_nithu59@rediffmail.com
Received March 5, 2011
Abstract—Ultrasonic velocity, density and viscosity of the ternary mixture of toluene + chloroform + cyclo-
hexane, were measured at 303.15, 308.15, and 313.15 K. The thermodynamically parameters such as adia-
batic compressibility (β), intermolecular free length (L
f
), free volume (V
f
), internal pressure (π
i
), acoustic
impedance (Z), molar sound velocity (R), and molar compressibility (W) have been obtained from the exper-
imental data for all the mixtures, with a view to investigate the exact nature of molecular interaction. Adia-
batic compressibility and intermolecular free length decrease with increase in concentration and tempera-
ture. The other parameters show almost increasing concentration of solutes. These parameters have been fur-
ther used to interpret the molecular interaction part of the solute and solvent in the mixtures.
Keywords: ultrasonic velocity, organic liquids, acoustical properties, molecular interactions.
DOI: 10.1134/S0036024412060295
PHYSICAL CHEMISTRY
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