Indian Journal of Novel Drug Delivery 5(4), Oct-Dec, 2013, 187-197
187
Indian Journal of Novel Drug Delivery
IJNDD
An Official Publication of
Karnataka Education and
Scientific Society
Research Article
Formulation and In-vitro Evaluation of Sustained Release Diclofenac
Sodium Matrix Tablets using Blends of Cashew Gum, Xanthan Gum and
Hydroxypropylmethylcellulose as Hydrophilic Drug Release Modifiers
K. OFORI-KWAKYE*, E. OBESE, M. E. BOAKYE-GYASI
Department of Pharmaceutics, Faculty of Pharmacy and Pharmaceutical Sciences, College of Health Sciences, Kwame Nkrumah
University of Science and Technology (KNUST), Kumasi, Ghana
A R T I C L E D E T A I L S A B S T R A C T
Article history:
Received on 18 October 2013
Modified on 25 November 2013
Accepted on 04 December 2013
Sustained release diclofenac sodium matrix tablets (~100 mg) were prepared by
wet granulation using blends of cashew gum, xanthan gum and HPMC as drug
release modifiers. The flow properties of diclofenac sodium granules and the
physical properties of the compressed matrix tablets namely, weight variation,
tablet thickness, crushing strength, friability, drug content and swelling index were
evaluated. In vitro dissolution studies were performed in phosphate buffer (pH 7.5)
using Voltaren Retard
®
tablet as a reference drug. Kinetic models and difference
(f1) and similarity (f2) factors were employed to evaluate the drug release data. The
granules exhibited good flow properties while the physical properties of tablets
generally fell within acceptable limits. Tablet formulations containing 60-100 %
xanthan gum exhibited high water absorption capacities in phosphate buffer pH
7.5. Formulations F10, F12, F13 and F15 passed the dissolution test for modified
release oral tablets while the rest failed the test. Formulations F7 to F15 appeared
similar to the reference drug (p < 0.05; f1 ≤ 10; f2 ≥ 60) and could be used
interchangeably. Drug release data fitted well to the Higuchi square root model and
the Korsmeyer-Peppas equation, indicating anomalous or non-Fickian drug release.
Blends of cashew gum, xanthan gum and HPMC when employed in the appropriate
ratios could optimize the sustained release activity of diclofenac sodium matrix
tablets.
© KESS All rights reserved
Keywords:
Natural gums,
Hydrophilic polymers,
Swelling capacity,
In vitro dissolution,
Sustained release
INTRODUCTION
Matrix tablets as monolithic systems have been
designed by various researchers as sustained
release drug delivery systems for oral
administration
[1-7]
. Other techniques which can
be used in the design of oral sustained release
products include the coating of beads, granules
and tablets with polymer materials; complex
formation; microencapsulation; and
extrusion/spheronization. Matrix drug delivery
systems may be produced using both hydrophilic
(e. g. HPMC, xanthan gum, sodium alginate) and
hydrophobic polymers (e. g. ethylcellulose,
polyvinyl chloride) and may be divided into lipid
matrix systems, inert or insoluble matrix systems
and hydrophilic matrix systems or swellable-
soluble systems.
Hydrophilic matrix tablets may be produced by
direct compression of the mixture of drug and
hydrophilic carriers
[8]
, or from a wet granulation
containing the drug and hydrophilic polymer
materials.
Cashew gum, xanthan gum and HPMC are
hydrophilic polymers which are used in matrix
tablet formulations as drug release modifiers for
controlled drug delivery
[9-12]
. Cashew gum is
obtained as exudates from the stem bark of the
tree Anacardium occidentale L. (family:
Anacardiaceae). It is naturally-occurring,
generally non-toxic, biocompatible and readily
available in many tropical and sub-tropical
countries. Cashew gum is a complex
polysaccharide of high molecular mass which
upon hydrolysis yields galactose and
galacturonic acid. Cashew gum has been utilized
as agglutinant for capsules and pills in the
pharmaceutical industry and in the food industry
as a stabilizer of juices. The binder and drug
*Author for Correspondence:
Email: koforikwakye@yahoo.com