Advances in solar photovoltaics are urgently needed to increase the performance and reduce the cost of harvesting solar
power. Solution-processed photovoltaics are cost-effective to manufacture and offer the potential for physical flexibility.
Rapid progress in their development has increased their solar-power conversion efficiencies. The nanometre (electron) and
micrometre (photon) scale interfaces between the crystalline domains that make up solution-processed solar cells are crucial
for efficient charge transport. These interfaces include large surface area junctions between photoelectron donors and accep-
tors, the intralayer grain boundaries within the absorber, and the interfaces between photoactive layers and the top and bottom
contacts. Controlling the collection and minimizing the trapping of charge carriers at these boundaries is crucial to efficiency.
Materials interface engineering for
solution-processed photovoltaics
Michael Graetzel
1
, René A. J. Janssen
2
, David B. Mitzi
3
& Edward H. Sargent
4
1
Institute of Photonics and Interfaces, Swiss Federal Institute of Technology, CH-1015 Lausanne, Switzerland.
2
Molecular Materials and Nanosystems, Eindhoven University of Technology, PO Box
513, 5600 MB Eindhoven, The Netherlands.
3
IBM TJ Watson Research Center, Yorktown Heights, New York 10598, USA.
4
Department of Electrical and Computer Engineering, University of Toronto,
Toronto, M5S 3G4, Canada.
O
ne hundred and twenty thousand terawatts of solar power
irradiate Earth. Globally, humans consume only 15 terawatts.
Solar power is abundant, free and can be harvested with mini-
mal effect on the environment.
The cost and efficiency of the solar cells that make use of this power
are of paramount importance. Single-crystal solar cells are formed
from a continuous piece of crystal, but solution-processed photovolta-
ics are manufactured on large, potentially flexible substrates (Fig. 1).
Light-absorbing and electrode materials are applied to the substrate by
techniques such as blade coating, spray coating, printing and slot-die
coating. Many solution-processing approaches use low temperatures,
reducing the energy cost associated with solar-cell manufacturing and
therefore the energy payback time. Lightweight, flexible solar modules
can also lower the installation and maintenance costs.
Four main families of solution-processed solar technologies are
approaching or have exceeded 10% solar-power conversion efficiency.
The challenge now is to continue this progress. Advances rely on con-
trolling the abundant materials interfaces that make up these highly
nanostructured devices. In this Review, we discuss the chemistry, phys-
ics and materials science of these interfaces, and their control through
materials chemistry. In particular, we focus on dye-sensitized solar cells
(DSSCs)
1
, organic photovoltaics
2
, solution-processed bulk inorganic
photovoltaics
3
and colloidal quantum-dot
4
solar cells.
The charge-separating junction is the boundary between two
intimately contacted materials at which photogenerated electron–
hole pairs are separated into longer-lived charge carriers (Fig. 2a, b).
Efficient operation of the solar cell relies on the separation and col-
lection of energy-bearing photocarriers before they lose their excess
energy through recombination. Typical diffusion lengths for the
performance-limiting photocarrier — minority charge carriers — are
within the 5–500-nm range in solution-processed semiconductors,
but the absorber thickness required to achieve complete absorption of
solar irradiation of interest is often considerably more than this. This
results in a possible trade-off between electron extraction and opti-
cal absorption if a planar absorber is used. To break this compromise,
solution-processed solar cells make use of highly nanostructured and
mesostructured interfaces.
Solution-processed photovoltaic materials generally contain signifi-
cant degrees of disorder, often because of the boundaries that define the
randomly orientated crystalline domains in both organic and inorganic
semiconductors. Transport within these domains, as well as at their
boundaries (including transport-limiting mechanisms, such as charge-
carrier trapping), requires attention and optimization.
One example of a beneficial boundary effect is the quantum
confinement of charge carriers to well-defined nanocrystalline domains,
such as in semiconductor quantum dots. This effect allows the tuning of
energy levels in materials. Wide-ranging tuning is advantageous because
the Sun emits such a broad spectrum of light (Fig. 2c). Relying on one
absorber bandgap limits the solar-cell power-conversion efficiency to
31% (ref. 5), whereas stacking cells with different bandgaps to create
multijunction configurations could increase the power-conversion
efficiencies to, in principle, a 68% limit (Fig. 2d).
We present the benefits of structured charge-separating interfaces and
review the chemical management of their electronic properties, discuss
interfaces within light-absorbing materials, describe the management
and characterization of these interfaces, and summarize the progress
and prospects in the field.
Morphology of charge-separating interfaces
DSSCs
6
(Fig. 3a) illustrate the use of nanostructured materials to
overcome weak absorption. A monolayer of sensitizer molecules
is anchored, with a linker, to an electron-accepting large-bandgap
semiconductor such as titanium oxide, tin oxide or zinc oxide. If the
monolayer was tethered to a planar electrode, it would absorb an insig-
nificant fraction of solar radiation (less than 1%). Instead, because
the electrode has a high-contact area, a three-dimensional junction is
formed with the metal-oxide nanoparticles. This nanostructured elec-
trode is many micrometres thick, and the dye–nanoparticle interface is
more than a thousand times the area of the solar cell.
Interfacial considerations are of particular concern in an architecture
in which every absorber molecule also forms one side of the charge-
separating junction. Four interfacial electron-transfer reactions have a
pivotal role in the efficiency of photoinduced charge separation. Injec-
tion of electrons from the dye into the conduction band of the oxide
nanoparticles must proceed faster than exciton recombination within
the dye. Recombination of forward-injected photoelectrons across
the dye–electrode interface must be prevented. The sensitizer must
be regenerated by donation of electrons from the electrolyte. Finally,
304 | NATURE | VOL 488 | 16 AUGUST 2012
REVIEW
doi:10.1038/nature11476
© 2012 Macmillan Publishers Limited. All rights reserved