Plasma Chemistry and Plasma Processing, Vol. 18, No. 3, 1998
Modeling of H2 and H2 /CH4 Moderate-Pressure
Microwave Plasma Used for Diamond Deposition1
K. Hassouni,2 O. Leroy, S. Farhat,2
and A. Gicquel2
Received October 8, 1997; revised December 4, 1997
One-dimensional transport models of moderate-pressure H2 and H2/CH4 plasmas
obtained in a diamond deposition microwave reactor are presented. These models
describe the plasma as a thermochemically nonequilibrium flow with three different
energy modes. The solution of the one-dimensional plasma transport equations
enabled the estimation of plasma species concentrations and temperatures on the
axis of the reactor. As far as pure H2 plasmas are concerned, results showed that
the model predictions of gas and vibration temperatures are in good agreement with
experimental measurements. The model also yields a relatively good qualitative
prediction of the variations of H-atom mole fraction with the power density absorbed
by the plasma. The results obtained for H2/CH4 discharges showed that the model
prediction on the variations of H-atom mole fraction with methane percentage in
the discharge is in good qualitative agreement with experimental results. They also
showed that methane is rapidly converted to acetylene before reaching the discharge
zone. The concentrations of neutral hydrocarbon species in the reactor are mainly
governed by thermal chemistry. The addition of methane strongly affects the ioniza-
tion kinetics of the plasma. Three major ions are generally obtained in H2/CH4
plasmas: C2H2, C 2 H3 , and C2 H5 . The relative predominance of these ions depends
on the considered plasma region and on the discharge conditions. The ionic species
concentrations are also mainly governed by chemistry, except very near the sub-
strate surface. Finally the use of this transport model along with the surface chem-
istry model of Goodwin(1) enabled us to estimate the diamond growth rate for several
discharge conditions.
KEY WORDS: Microwave plasma; diamond deposition; modeling.
1. INTRODUCTION
Moderate-pressure H2/CH4 microwave plasmas are now routinely used
for the chemical vapor deposition of diamond films. Usually, the deposition
process is characterized by a pressure ranging between 20 and 120 torr, an
1invited lecture presented at the 13th International Symposium on Plasma Chemistry, Beijing,
PRC, August 18-22, 1997.
2LIMHP, CNRS-UPN, Avenue 3. B. Clement 93430 Villetaneuse, France.
325
0272-4324/98/0900-0325$15.00/0 © 1998 Plenum Publishing Corporation