IJSRSET173474 | Received : 20 July 2017 | Accepted : 01 August July- 2017 | July-August-2017 [(3)5: 296-299 ]
© 2017 IJSRSET | Volume 3 | Issue 5 | Print ISSN: 2395-1990 | Online ISSN : 2394-4099
Themed Section: Engineering and Technology
296
Vibrational (UV and NMR) Analysis of 4-(Trifluoromethoxy)
benzylbromide by Density Functional Theory Calculations
S.P. Saravanan
a
, A. Sankar
b
and K. Parimala
c
a
Department of Chemistry, Vivekanandha Arts and Science College for Women, Sankari, India
b
Department of Chemistry, Kandaswami Kandar's College, P.Velur, India
c
Department of Physics, Vivekanandha College of Arts and Sciences for women (Autonomous), Namakkal, India
ABSTRACT
The energy and oscillator strength are calculated by time-dependent density functional theory (TD-DFT) with the
experimental findings for 4-(Trifluoromethoxy) benzylbromide (TMB).
13
C and
1
H NMR chemical shifts results
were also compared with the experimental values. Both UV and NMR shielding values calculated using LSDA
method with 3-21G basis set.
Keywords: TMB, NMR, LSDA.
Corresponding Author: +91 9443828391
E-mail address: spschemistry1977@gmail.com (S.P. Saravanan)
I. INTRODUCTION
Benzyl bromide’s production and use as a foaming and
frothing agent and in organic synthesis may result in its
release to the environment through various waste
streams. Benzyl bromide may be release to air in
automobile exhaust from vehicles using leaded gasoline
containing ethylene dibromide (a lead scavenger). If
released to air, a vapor pressure of 0.45 mmHg at 25˚C
indicates benzyl bromide will exist solely as a vapor in
the ambient atmosphere. Vapor-phase benzyl bromide
will be degraded in the atmosphere by reaction with
photochemical-produced hydroxyl radicals; the half-life
for this reaction in air is estimated to be 7 days. If
released to soil, benzyl bromide is expected to have low
mobility based upon an estimated Koc of 920. However,
mobility in soil may be mitigated based on the
hydrolysis of benzyl bromide in water.
Benzyl bromide is expected to undergo chemical
hydrolysis in water and moist soil based on a hydrolysis
half-life of 79 min thus volatilization from water
surfaces, bio concentration in aquatic organisms, and
sorption to suspended solids and sediment are not
expected to be important fate processes. Occupational
exposure to benzyl bromide may occur through
inhalation and dermal contact with this compound at
workplaces where benzyl bromide is produced or used.
Monitoring data indicated that the general population
may have been exposed to benzyl bromide via
inhalation of automobile exhaust from vehicles using
leaded gasoline.
Bromophenyl methane is also known as a bromotoluene
or benzyl bromide. It is a corrosive clear, water
insoluble liquid with a typical smell of paint thinners,
redolent of the sweet smell of the related compound
benzene. It can be prepared by the bromination of
toluene at room temperature in air, using manganese (IV)
oxide as a heterogeneous catalyst. It is used in organic
synthesis for the introduction of the benzyl protecting
group for alcohols and carboxylic acids. It is an
aromatic hydrocarbon that is widely used as an
industrial feed stock and as a solvent. It is also a
common solvent, able to dissolve paints, paint thinners,
many chemical reactants, rubber, painting ink, glues,
lacquers, leather tanners, many disinfectants and a
useful raw material for certain important products such
as poly urethane foam, phenol and TNT.
In addition, toluene can be used as fullerene indicator
and an octant booster in gasoline fuels used in internal