Modeling the aggregation of partially covered particles: Theory and simulation A. Moncho-Jorda ´ , 1, * G. Odriozola, 2,² M. Tirado-Miranda, 3,‡ A. Schmitt, 1,§ and R. Hidalgo-A ´ lvarez 1, 1 Departamento de Fı ´sica Aplicada, Universidad de Granada, Campus Fuentenueva, E-18071 Granada, Spain 2 Programa de Ingenierı ´a Molecular, Instituto Mexicano del Petro ´leo, La ´zaro Ca ´rdenas 152, 07730 Me ´xico, Distrito Federal, Mexico 3 Departamento de Fı ´sica, Escuela Polite ´cnica, Universidad de Extremadura, Avenida de la Universidad, 10071 Ca ´ceres, Spain Received 2 February 2003; published 15 July 2003 A theoretical model for describing the initial stages of the aggregation of partially covered colloidal particles is presented. It is based on the assumption of short-range interactions that may be modeled by a sticking probability on contact. Three types of sticking probabilities are distinguished depending on the collision type, i.e., for bare-bare, bare-covered, and covered-covered collisions. Hence, the model allows an analytical ex- pression for the dimer-formation rate constant k 11 , to be deduced as a function of the degree of surface coverage and the three sticking probabilities. The theoretical predictions are contrasted with simulated data. The observed agreement between theory and simulations shows the usefulness of the model for predicting the initial stages of this kind of aggregation processes. DOI: 10.1103/PhysRevE.68.011404 PACS numbers: 61.43.Hv, 02.50.-r, 82.70.Dd, 05.40.Jc I. INTRODUCTION Macromolecules adsorbed onto colloidal particle surfaces may either stabilize or destabilize the dispersions. This makes the employment of macromolecules as additives for suspensions a much extended practice for industrial pur- poses. Several applications can be found in mineral and waste water treatments, such as water treatments for human consumption, paper industry, drilling fluids, ceramics, agro- chemical formulation, and in immunoassay diagnostic test design 1. However, such processes are so highly complex in nature that they have not been completely understood, yet. Given any particular situation where macromolecules and colloidal particles are taking part, the process will depend on the degree of surface coverage with macromolecules and on the macromolecule-macromolecule and macromolecule- particle interactions 2,3. When the particle surface is fully covered by the macromolecules, the observed result is gen- erally a stabilized suspension 4,5. For partially covered sur- faces, however, the already adsorbed macromolecules on a given particle may attach to the bare patch of another one forming a particle-particle bridge bridging flocculation 6,7. It is well known that the bridging flocculation rate de- pends on the degree of surface coverage. The classical work of La Mer and Healy 8predicts a maximum of the floccu- lation rate when half the total surface is covered by macro- molecules. When additional factors contribute to destabiliza- tion, the optimum degree of surface coverage usually becomes smaller 9. In spite of the large amount of experimental work that has been performed for studying different aspects of these types of systems 10–18, there is still a lack of theoretical models for explaining their flocculation kinetics. In this work we attempt to fill this gap proposing a model based on La Mer’s idea of a surface coverage dependent aggregation rate ca- pable of describing the initial stages of an aggregation pro- cess. Additionally, the concepts of sticking probability and consecutive collisions recently employed for modeling the transition from diffusion to reaction limited cluster aggrega- tion are also included 19,20. The obtained results are then compared with Brownian dynamics simulations. The paper is organized as follows. Section II reports the theoretical background. Section III briefly describes the simulations, presents some simulation results, and confirms that the models found in the literature are not capable of matching the data. In Sec. IV an alternative model is pro- posed and its predictions are compared with the simulated data. Finally, Sec. V tackles the conclusions. II. THEORETICAL BACKGROUND Colloidal aggregation processes may be monitored by the time evolution of the cluster concentrations, c i ( t ) =n i ( t )/ V , where n i ( t ) is defined as the number of clusters of size i at time t, and V is the whole volume where the aggregation takes place. For dilute systems the time evolu- tion of the cluster concentrations is given by the Smolu- chowski equation 21,22: dc i dt = 1 2 j =1 i -1 k j , i - j c j t c i - j t -c i t j =1 k ij c j t . 1 The kinetic rate constants, or the aggregation kernel, k ij , represent the mean rate at which two i- and j-size clusters stick to form a ( i + j )-size cluster. It contains all physical information about the kinetics of the aggregating system. The cluster concentrations c i ( t ) are average quantities that do not consider the internal cluster structure. Nevertheless, this information is implicitly included in the size dependence of the kernel k ij . It should be noted that the kernel is an orientational and morphological average of all particular cluster formation possibilities. *Email address: moncho@ugr.es ² Email address: godriozo@imp.mx Email address: mtirado@ugr.es § Email address: schmitt@ugr.es Email address: rhidalgo@ugr.es PHYSICAL REVIEW E 68, 011404 2003 1063-651X/2003/681/01140412/$20.00 ©2003 The American Physical Society 68 011404-1