Food Biotechnology, 26:143–153, 2012
Copyright © Taylor & Francis Group, LLC
ISSN: 0890-5436 print / 1532-4249 online
DOI: 10.1080/08905436.2012.670829
Cloning, Expression,
Purification and Refolding
of Caprine Prochymosin
Mohammad Hadi Eskandari
1
, Arsalan Hosseini
2
,
Sepideh Alasvand Zarasvand
1
, and Mahmoud Aminlari
3
1
Department of Food Science and Technology, College of Agriculture, Shiraz
University, Shiraz, Iran
2
Department of Pathobiology, School of Veterinary Medicine, Shiraz University,
Shiraz, Iran
3
Department of Biochemistry, School of Veterinary Medicine, Shiraz University,
Shiraz, Iran
Chymosin is an aspartic proteinase found in the stomach of neonatal mammals and
is used as milk coagulant in the cheese industry. In this study, preprochymosin cDNA
from the abomasums of Iranian natives’ kid goats was cloned and characterized. This
cDNA has an open reading frame of 1143 bp and is predicted to code for a preproenzyme
of 381 amino acids with an N-terminal 16 amino acid signal peptide that is followed by
a 42 amino acid proenzyme. The deduced amino acid sequence revealed 98.7% and 94%
identity with corresponding lamb and cattle sequences, respectively. The cDNA encod-
ing for prochymosin was then subcloned into pET-28a and expressed with and without
N-terminal His-tag in E. coli BL
21
(DE
3
). Inclusion bodies were isolated and solubilized
in 8 M urea at pH 10.7. Solubilized prochymosion molecules were successfully refolded
and active recombinant goat chymosin was recovered after subsequent activation. Milk
clotting activity (416 U/mg and 192 U/mg) was observed in (His
+
)-prochymosin and
(His
-
)-prochymosin enzymes, respectively, after activation.
Key Word: caprine; recombinant prochymosin; His-tag; activity
INTRODUCTION
Chymosin (rennin; E.C. 3.4.23.4), an aspartic proteinase normally present in
the stomach of all nursing mammals and is used as the major milk clotting
enzyme in the cheese industry (Chitpinityol and Crabbe, 1998). Chymosin
is secreted as a zymogen called prochymosin, which consists of a single
Address correspondence to Mohammad Hadi Eskandari, Department of Food Science
and Technology, College of Agriculture, Shiraz University, Shiraz, Iran; E-mail:
eskandar@shirazu.ac.ir