Anti-inammatory signaling actions of electrophilic nitro-arachidonic acid in vascular cells and astrocytes * Andr es Trostchansky, Homero Rubbo * Departamento de Bioquímica and Center for Free Radical and Biomedical Research, Facultad de Medicina, Avda. General Flores 2125, Universidad de la República, Montevideo 11800, Uruguay article info Article history: Received 22 August 2016 Received in revised form 28 September 2016 Accepted 3 October 2016 Available online xxx Keywords: Nitro-arachidonic acid Lipid nitration Platelets Macrophages Inammation Electrophilic signaling abstract Nitrated derivatives of unsaturated fatty acids (nitro-fatty acids) are being formed and detected in human plasma, cell membranes and tissue, triggering signaling cascades via covalent and reversible post- translational modications of nucleophilic amino acids in transcriptional regulatory proteins. Arach- idonic acid (AA) represents a precursor of potent signaling molecules, i.e., prostaglandins and throm- boxanes through enzymatic and non-enzymatic oxidative pathways. Arachidonic acid can be nitrated by reactive nitrogen species leading to the formation of nitro-arachidonic acid (NO 2 -AA). A critical issue is the inuence of NO 2 -AA on prostaglandin endoperoxide H synthases, modulating inammatory pro- cesses through redirection of AA metabolism and signaling. In this prospective article, we describe the key chemical and biochemical actions of NO 2 -AA in vascular and astrocytes. This includes the ability of NO 2 -AA to mediate unique redox signaling anti-inammatory actions along with its therapeutic potential. © 2016 Elsevier Inc. All rights reserved. 1. Introduction Free as well as esteried fatty acids are important components of biological membranes that can be modied by reactive oxygen (ROS) and nitrogen (RNS) species. Nitration of fatty acids is ex- pected to occur in hydrophobic compartments such as the lipid bilayer of cellular membranes or the lipophilic core of lipoproteins. It is well reported that RNS both oxidize and nitrate unsaturated fatty acids yielding an array of hydroxyl, hydroperoxy, nitro and nitrohydroxy derivatives [1], with the in vivo mechanism for nitro- fatty acid (NO 2 -FA) formation still remain unknown. Most of the available work suggests the presence of nitrogen dioxide ( NO 2 ) as the limiting step, being its most probable source nitric oxide ( NO) autooxidation [2]. Also, NO 2 can be generated from the decom- position of peroxynitrite, peroxidase-catalyzed oxidation of nitrite (NO 2 ) to NO 2 or reduction of NO 2 in acidic tissue environments (e.g., gastric compartment, ref. [3]). In fact, NO and superoxide radical (O 2 ) are the precursors of peroxynitrite which under inammatory conditions where it is observed an increase of either oxidized and nitrated proteins and lipids [4]. Since both perox- ynitrite and NO 2 readily diffuse through the membrane bilayers, reactions leading to NO 2 generation may take place in the aqueous environment in proximity to the membrane or inside the lipid bilayer [5]. Inammatory related diseases (e.g. atherosclerosis, diabetes) present an increase of both ROS and RNS formation as well as the participation of macrophages and platelets in many of the patho- logical states derived from the activation of inammatory processes [6e9]. Both cell types have an active participation of arachidonic acid (AA) metabolizing pathway with the formation of pro- and anti-inammatory eicosanoids as well as formation of ROS and RNS and changes in the cell redox status [10e13]. The aim of this review is to discuss the biological effects of the addition of a nitro group (-NO 2 ) to the carbon chain of AA in platelets, macrophages and astrocytes. Modulation of pro- and anti-inammatory enzymes by nitroarachidonic acid (NO 2 -AA) as well as key cellular signaling pathways are detailed. 1.1. Enzymatic oxidation of arachidonic acid Arachidonic acid (20:4) is the precursor of many biologically- and physiologically-relevant bioactive lipids, being its cellular * This article is part of a Special Issue entitled The Chemistry of Redox Signaling, edited by Henry Forman and Willem H. Koppenol. * Corresponding author. Avda. General Flores 2125, CP 11800, Montevideo, Uruguay. E-mail address: hrubbo@fmed.edu.uy (H. Rubbo). Contents lists available at ScienceDirect Archives of Biochemistry and Biophysics journal homepage: www.elsevier.com/locate/yabbi http://dx.doi.org/10.1016/j.abb.2016.10.003 0003-9861/© 2016 Elsevier Inc. All rights reserved. Archives of Biochemistry and Biophysics xxx (2016) 1e7 Please cite this article in press as: A. Trostchansky, H. Rubbo, Anti-inammatory signaling actions of electrophilic nitro-arachidonic acid in vascular cells and astrocytes, Archives of Biochemistry and Biophysics (2016), http://dx.doi.org/10.1016/j.abb.2016.10.003