Molecular dynamics simulation of icosahedral Si quantum dot formation from liquid droplets Kengo Nishio,* Tetsuya Morishita, Wataru Shinoda, and Masuhiro Mikami Research Institute for Computational Sciences (RICS), National Institute of Advanced Industrial Science and Technology (AIST), Central 2, Umezono 1-1-1, Tsukuba, Ibaraki 305-8568, Japan Received 31 August 2005; published 15 December 2005 The present paper reports on molecular dynamics simulations of the formation process of Si quantum dots Si QDs. Icosahedral Si QDs are formed spontaneously by freezing 274-, 280-, and 323-atom Si droplets. We find that the initialization of pentagonal channels leads into the overall icosahedral structure. We also study the melting behavior of the 280-atom icosahedral Si QD. We find that the melting point is reduced more than 15% compared with that of bulk Si. A possible approach to synthesize icosahedral Si QDs is discussed. The formation of the icosahedral structure could be expected in other systems characterized by tetrahedral bonding network. DOI: 10.1103/PhysRevB.72.245321 PACS numbers: 78.67.Hc, 65.80.+n, 81.07.Ta I. INTRODUCTION Silicon quantum dots Si QDsare scientifically and tech- nologically important semiconductor nanoparticles. Their op- tical properties and electronic structures vary dramatically with size and atomic arrangement. 1–7 For example, the peak position of photoluminescence can be tuned by controlling the size, and the intensity of photoluminescence is higher in amorphous Si QDs than in crystalline Si QDs. 4,5 It has also been suggested that the spin dephasing time and coherence in optical excitations can be tuned by controlling the symmetry of the atomic arrangement. 7 These facts stress the importance of understanding and controlling the structure of Si QDs. While the most stable structures are well understood in small Si particles by theoretical calculations, 8,9 the determination of the structures in the nanosize regime is a very hard task. 7,10,11 The most stable morphology of rare gas, gold, and copper nanoparticles changes from fcc to decahedral to icosahedral, as the size decreases. 12–17 For Si, one can draw two analo- gies. First, the space lattice of bulk crystalline Si is fcc. Sec- ond, although the yield is quite low, decahedral Si QDs have been observed in samples prepared by the gas evaporation method. 18,19 It is then expected that small Si QDs can be formed in the icosahedral structure. From a geometrical viewpoint, the icosahedral structure, which consists of 20 slightly distorted crystalline tetrahedra, each exposing one of four 111facets, can be built in the framework of tetrahedral bonding. 20 The 111facets have the lowest area density of dangling bonds so that the surface energy could be minimum. The stability of the icosahedral structure at 0 K is determined by the competition of the strain energy and the surface energy. Recent first-principles calculations have shown that icosahedral Si QDs i-Si QDs have lower structure energies than crystalline Si QDs c-Si QDsat least for diameters smaller than 2.77 nm. 7 However it is not clear whether such a structure really exists. Previous theoretical and experimental studies in various systems have suggested that the formation process actually determines the morphology of a nanoparticle. 5,6,12–14,16,18,19,21 For example, by controlling experimental conditions, c-Si QDs or amorphous Si QDs can be selectively synthesized. 5,6 Given the situation, molecular dynamics MDsimulation is a powerful technique to study the stable structure of Si QDs 11,12,14,21 because it enables us to investigate the forma- tion process of Si QDs directly by following up the motion of Si atoms. In addition, the thermal stability of Si QDs can be investigated. In the present paper, we study the formation process of Si QDs of diameters in the range of 2.17 to 2.31 nm by means of MD simulations. Long-time simulations show that i-Si QDs are formed spontaneously by freezing Si droplets. The formation of pentagonal channels plays an important role in the formation of i-Si QDs. We also find that the melting point of the i-Si QD of 2.20 nm in diameter is reduced more than 15% compared with that of bulk Si. II. MODEL AND METHODS As we shall show later, it takes more than 50 ns to pro- duce i-Si QDs by freezing Si droplets. Phenomena of such a long time-scale are intractable via first-principles or tight- binding molecular dynamics TBMDsimulations. A short time-scale simulation by the TBMD method has shown that a 281-atom Si droplet freezes into an amorphous Si QD, 11 that is, the system is trapped in some metastable state. In our MD simulations, Si atoms are modeled by the empirical Tersoff potential, which is known to reproduce structural properties well, including tetrahedral bonding networks in both crystal- line and amorphous phases. 22–24 By choosing the empirical potential, we can perform simulations long enough to study the formation process of i-Si QDs. When one uses empirical potentials, it is necessary to consider the transferability of the potentials. We consider that the Tersoff model captures the essence for representing the structural properties of i-Si QDs from the following two physical insights based on the results of the first-principles calculations: 7 1i-Si QDs are con- structed by covalent bonding, or tetrahedral bonding not by metallic bonding which is observed in very small clusters; 2the poor description of the energetics of surface recon- structions in the Tersoff model does not affect the overall icosahedral structure, because i-Si QDs expose 111facets without surface reconstructions. PHYSICAL REVIEW B 72, 245321 2005 1098-0121/2005/7224/2453214/$23.00 ©2005 The American Physical Society 245321-1