EFFECT OF HEAT TREATMENT ON MECHANICAL PROPERTIES OF LAMINATED CARBON FIBER
REINFORCED POLYMERIC COMPOSITES
ABM I. Islam
Department of Nanoengineering, JSNN,
North Carolina A&T State University
Greensboro, North Carolina, USA
aiislam@aggies.ncat.edu
Ajit D. Kelkar
Department of Nanoengineering, JSNN,
North Carolina A&T State University
Greensboro, North Carolina, USA
kelkar@ncat.edu
Lifeng Zhang
Department of Nanoengineering, JSNN,
North Carolina A&T State University
Greensboro, North Carolina, USA
lzhang@ncat.edu
ABSTRACT
In recent years use of electrospun nanofibers and
nanoparticles to improve the interlaminar properties have
increased significantly. In most of the cases the additional
interlaminar phase of nanofibers is required to go through
various thermal and/or chemical processes. There has been
emphasis to optimize the interlaminar nanofiber layers to
achieve the optimum desired mechanical properties such as
interlaminar strength. One common practice is to disperse
nanofibers into the resin and then use the nanofiber enhanced
resin to fabricate the laminated composites. However, proper
dispersion and fiber filtering out are some of the problems that
exist in fabrication using the nanofiber mixed resin approach. To
alleviate this problem, an innovative approach of growing PAN
(polyacrylnitrile) nano fibers directly on carbon fabric by
electrospinning seems to solve the dispersion and fiber filtering
problem. However, as PAN fibers require stabilization and
carbonization, it is obvious that carbon fabric with PAN fiber
deposition will have to undergo stabilization and carbonization
process. The effect of stabilization and carbonization heat
treatment on the mechanical properties of carbon fiber fabric is
not yet fully understood. This paper presents the effects of heat
treatment on carbon fabric used for fabricating laminated carbon
fiber reinforced composite with epoxy resin. The heat treatment
was performed at 280
o
C in air for six hours, and 1200
o
C for one
hour in nitrogen which are similar to stabilization and
carbonization of pure PAN fibers. The effects, due to heat
treatment, were mainly characterized in terms of mechanical
properties by performing tensile tests and shear tests. Fiber
surface topography was observed by SEM to analyze physical
changes. Chemical changes, corresponding to the existing
groups with carbon fibers, were examined through FTIR. The
results obtained are compared with a set of control laminated
composite specimens, which were fabricated using heat vacuum
assisted resin transfer molding (HVARTM) process and cured at
149
o
C. The two sets of composite were infused with resin in a
single vacuum bag to ensure that both sets of specimens have
identical resin infusion and cure cycle. Laminates used for
making control specimens were fabricated using carbon fabric
which did not undergo any heat treatment. A change in laminate
thickness for heat treated carbon fabric was observed indicating
a possible bulk up of the carbon fibers due to loss of sizing
compounds, which also resulted into significant change in tensile
properties.
INTRODUCTION
It is recognized that nanomaterials have significant potential
for increasing interlaminar strength of the composite. However,
to scale up from the laboratory practice to commercial
production is a great challenge. The first and the most common
approach for introduction of the nanomaterial, in composite
applications, is dispersing them into the resin. Many researchers
premixed nanofibers with resin and used the mixture of
nanofiber filled resin for resin transfer molding or resin infusion
to fiber preform. The major problem arises while using the
nanoparticles or nanofibers using the dispersion process, is the
increased in the viscosity of the resin, which makes it difficult to
flow [1]. Therefore, the proper penetration through the fiber mats
Proceedings of the ASME 2016 International Mechanical Engineering Congress and Exposition
IMECE2016
November 11-17, 2016, Phoenix, Arizona, USA
IMECE2016-65206
1 Copyright © 2016 by ASME
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