IJSRST1845472 | Received : 05 April 2018 | Accepted : 23 April 2018 | March-April-2018 [ (4) 5 : 1636-1640]
© 2018 IJSRST | Volume 4 | Issue 5 | Print ISSN: 2395-6011 | Online ISSN: 2395-602X
Themed Section: Science and Technology
1636
Green Synthesis and Characterization of ZnO- Ag Nanocomposite
by Thymus vulgaris
Mina Zare
1,2
, K. Namratha
1,2
, K.Byrappa
1,2
*
1
DOS in Earth Science, Mansagangothri, University of Mysore, Mysore, India
2
Centre for Materials Science and Technology, Vijnana Bhavana, University of Mysore, Mysore, India
*Corresponding author: kbyrappa@gmail.com
ABSTRACT
In this study, ZnO-Ag nanocomposite (NCs) was synthesized less than 20 nm through a simple and eco-friendly
bio-hydrothermal method by using aqueous Thymus vulgaris (Thyme) leaf extract. Thyme leaf extract was used
as a reducing agent and surfactant in the green synthesis of ZnO-Ag NCs. Crystal structure, Functional group,
morphology, chemical elemental, the band gap of ZnO-Ag NCs were characterized by using powder X-ray
diffraction, Fourier Transform Infrared Spectroscopy, Transmission Electron Microscopy, Energy Dispersive X-
ray analysis, UV-visible spectroscopy, respectively. TEM results confirmed the size and morphology of
nanocomposite. The influence of silver nitrate concentration in the formation of ZnO-Ag NCs was studied. This
study future aims that to use biocompatible ZnO-Ag nanocomposite for biological application and food
packaging.
Keywords: Hydrothermal synthesis, Thyme leaf extract, ZnO-Ag Nanocomposite, Characterization
I. INTRODUCTION
Metal and metal oxide nanoparticles are
interesting because of their great optical, chemical,
electrical and magnetic properties [1]. These
properties bring the materials interesting in different
application areas, including nanoelectronics devices,
catalysis, nonlinear optical devices, bio-medical, etc
[2]. Metal oxides semiconductor nanocomposites have
been widely explored due to their potential
applications in various fields [3].
Between metal and metal oxides, Ag and ZnO
nanoparticles have attracted large attention, not only
because ZnO has great chemical stability, low cast,
large surface area and wide-band gap with various
applications, including use in electronics, solar cells,
photo electronics and sensors, but also because Ag
nanomaterials illustrate some unique features in
biological and chemical sensing and high electrical
conductivity. Additionally, Ag modification is found
to be effective for the synthesis of p-type ZnO, as the
naturally occurring ZnO demonstrations n-type
conductivity as a result of its innate defects such as
oxygen vacancies and zinc interstitials [4] . Recently,
Ag ions become more attracts of the several research
works, due to their novel effects on the evolution of
antibacterial activity and efficiency of photo catalytic
activity of semiconductor [5].
On the other hand, recently zinc oxide
nanoparticles has received much consideration due to
it has a vast range of attributes that depend on doping,
with a range of conductivity from metallic to