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ISSN 1063-7834, Physics of the Solid State, 2018, Vol. 60, No. 6, pp. 1158–1162. © Pleiades Publishing, Ltd., 2018.
Original Russian Text © I.A. Baraban, A.V. Emelyanov, P.N. Medvedskaya, V.V. Rodionova, 2018, published in Fizika Tverdogo Tela, 2018, Vol. 60, No. 6, pp. 1147–1151.
Low Temperature Magnetic Properties
of Amorphous Ferromagnetic Fe–Si–B Glass-Coated
and Glass Removed Microwire
1
I. A. Baraban
a
, A. V. Emelyanov
b
, P. N. Medvedskaya
a
, and V. V. Rodionova
a,
*
a
Immanuel Kant Baltic Federal University, Kaliningrad, 234041 Russia
b
National Research Center “Kurchatov Institute,” Moscow, 123182 Russia
*e-mail: rodionova@lnmm.ru
Received December 25, 2017
Abstract—This work presents results of investigations of low temperature magnetic properties of microwires,
fabricated by the Ulitovsky–Taylor method from Fe–Si–B alloy. Influence of the glass coating presence on
the magnetostatic properties was shown at room temperature and at 2 K. Conclusions about the peculiarities
of temperature dependence of the magnetic moment, measured in low and high magnetic fields (10 Oe–
5 kOe) in the temperature range from 2 to 300 K for a sample with partially reduced fabricated process-
induced stress by removing the glass, were made.
DOI: 10.1134/S1063783418060070
1. INTRODUCTION
Amorphous ferromagnetic glass-coated microw-
ires with Fe-based metallic nucleus exhibit properties
of magnetic bistability in a wide range of their dimen-
sions—both the transverse [1–3] and longitudinal [4–
6], as well as in a wide temperature range [7–9]. Mag-
netic bistability opens a lot of prospects for the practi-
cal use for microwires, for example, as a sense element
of sensors of various physical quantities (stress, tem-
perature, magnetic field, and others) [10, 11], as a
functional element of the coding and reading systems
[12, 13].
The nature of the magnetic bistability of glass-
coated amorphous ferromagnetic microwires is in the
micromagnetic structure—Landau–Lifshitz [14],
formed during the process of microwires manufactur-
ing by the Ulitovsky–Taylor method. In this case, a
large volume of the metallic nucleus is occupied by an
axially magnetized core, and a small volume on the
periphery has a domain structure with a radially
directed axis of easy magnetization [15]. The volume
of closure domains, arising in the microwire due to the
system’s aiming to minimize the magnetostatic
energy, depends, first of all, on the demagnetizing
field of microwire and essentially increases with an
increase of the form factor of the sample (a decrease in
the length or increase in diameter at a fixed second
parameter) [6].
Magnetoelastic energy, K
me
~ 3/2λ
S
σ, plays a cru-
cial role in the formation of micromagnetic structure
and, consequently, of magnetic properties of the
metallic nucleus of a glass-coated microwire (because
transverse dimensions of the sample are much smaller
than its longitudinal dimensions and the material of
the metallic nucleus is amorphous, the magnetostatic
energy and magnetocrystalline energy, respectively,
can be neglected) [16]. Therefore, the direction of the
mechanical stress σ and the sign of the magnetostric-
tion coefficient λ
S
determine the direction of the easy
magnetization axis. Mechanical stresses σ are induced
in the metallic nucleus of the microwire during the
Ulitovsky–Taylor technique, because of the fast
quenching process, difference in the thermal expan-
sion coefficients of the metal and glass, and of the
applied mechanical tensile stress (drawing). Radial
distribution of the components σ
ii
of the mechanical
stress tensor of the metallic nucleus is formed in such
a way that the tensile stresses are dominant in a larger
volume of the metallic nucleus of the wire (up to
0.95d/D, where d is the diameter of the metallic
nucleus of the microwire, and D is the total diameter
of the microwire in the glass shell) [16, 17]. Therefore,
to form a Landau–Lifshitz-wise structure where an
axially magnetized core occupies a larger volume of
the metallic nucleus, it is sufficient to select for fabri-
cation a high magnetostrictive material with a positive
magnetostriction coefficient λ
S
, for example Fe–Si–
B. In this case, the metallic nucleus of the microwire
can be considered as a single domain (at sufficient
1
The article was translated by the authors.
MAGNETISM