ISSN 1063-7842, Technical Physics, 2013, Vol. 58, No. 10, pp. 1432–1436. © Pleiades Publishing, Ltd., 2013.
Original Russian Text © V.I. Betekhtin, Yu.R. Kolobov, O.A. Golosova, B.K. Kardashev, A.G. Kadomtsev, M.V. Narykova, M.B. Ivanov, T.N. Vershinina, 2013, published in Zhurnal
Tekhnicheskoi Fiziki, 2013, Vol. 83, No. 10, pp. 38–43.
1432
INTRODUCTION
Interest in titanium and titanium-based alloys is
caused by a unique combination of its properties,
namely, a high strength, a low density, and a low elastic
modulus. The last feature is important for developing
biomedical alloys, since such materials must have both
biochemical compatibility with human being tissues,
which consists in the absence of immune reactions and
inflammatory processes, and biomechanical compati-
bility, which determines the functional reliability of
implants [1–4]. The main characteristic of the biome-
chanical compatibility of an implanted material is the
elastic modulus, which should be as close as possible to
the elastic modulus of the bone (30 GPa). This close-
ness makes it possible to avoid the so-called stress-
shielding effect, which manifests itself in inevitable
bone resorption (bone dissolution because of osteo-
clast activity) in the region without mechanical loads
and, in contrast, at the sites of excess stress and strain
concentrations (which are higher than those typical of
normal functioning of bone structures) [5].
From this standpoint, titanium β alloys with a low
elastic modulus, which is close to that of the bone tis-
sue, are of particular interest for application as a mate-
rial for implantology [3, 6]. A decrease in the elastic
modulus of titanium alloys is achieved by introducing
a set of certain β-stabilizing alloying elements except
for V, Al, Ni, and Co, which exert an allergic action on
living tissues or a general toxic action on a human
being [1, 7, 8]. At present, alloying with niobium,
molybdenum, and zirconium is most promising. Tita-
nium-based alloys with these elements have a low elas-
tic modulus, a high corrosion resistance, and a
mechanical strength sufficient for most applications;
in addition, they are ductile and manufacturable [9].
The purpose of this work is to study the effect of
thermomechanical treatment (rolling followed by
annealing) on the elastic modulus, the amplitude-
independent damping ratio, the microplastic flow
stress, and the density of a Ti–26Nb–7Mo–12Zr tita-
nium β alloy using an acoustic resonance method and
densimetry.
EXPERIMENTAL
As a starting material, we chose a titanium β alloy
containing 55% Ti, 26% Nb, 7% Mo, and 12% Zr (Ti–
26Nb–7Mo–12Zr) with an average grain size of 280 ±
9 μm; it was fabricated by vacuum arc remelting at
OAO VSMPO-AVISMA (Verkhnyaya Salda, Russia)
followed by forging at temperatures above the recrys-
tallization temperature.
The thermomechanical treatment (TMT) of the
alloy consisted in sheet rolling followed by recrystalli-
zation annealing. Rolling was performed without
heating (at room temperature) at a reduction of 100–
200 μm per pass to a total reduction of 30, 60, and
90%. The prepared samples were subjected to anneal-
ing at 850°C followed by water quenching.
To study the elastoplastic properties, we used an
acoustic resonance method performed with a com-
pound piezoelectric vibrator at a longitudinal vibra-
tion frequency of about 100 kHz. The elastic modulus
and the amplitude-independent damping ratio were
measured over a wide vibrational strain amplitude
range. We used moderate amplitudes to retain the dis-
location structure of the samples: after acoustic
Elastoplastic Properties
of a Low-Modulus Titanium-Based β Alloy
V. I. Betekhtin
a
*, Yu. R. Kolobov
b, c
, O. A. Golosova
b
, B. K. Kardashev
a
, A. G. Kadomtsev
a
,
M. V. Narykova
a
, M. B. Ivanov
b
, and T. N. Vershinina
b
a
Ioffe Physical Technical Institute, Russian Academy of Sciences, Politekhnicheskaya ul. 26, St. Petersburg, 194021 Russia
*e-mail: Vladimir.Betekhtin@mail.ioffe.ru
b
Research–Educational Center Nanostructured Materials and Nanotechnologies, Belgorod State University,
ul. Pobedy 85, Belgorod, 308015 Russia
c
Institute of Problems of Chemical Physics, Russian Academy of Sciences, Chernogolovka, Moscow oblast, 142432 Russia
Received September 10, 2012; in final form, December 19, 2012
Abstract—The elastoplastic properties (elastic modulus, amplitude-independent damping ratio, microplas-
tic flow stress) of a Ti–26Nb–7Mo–12Zr titanium β alloy are determined using an acoustic resonance
method. The effect of the strain during thermomechanical treatment on the structural features of the micro-
crystalline alloy and, hence, its elastoplastic properties is analyzed.
DOI: 10.1134/S1063784213100046
SOLID
STATE