Applied Surface Science 43 (1989) 237-241 237
North-Holland
EFFECTS ON THE IMPLANTED PROFILES OF POINT DEFECT FLUX
DURING NITROGEN IMPLANTATION IN COPPER
D.C. KOTHARI
Istituto per la Ricerca Scientifica e Tecnologica, 1-38050 Povo, Trento, Italy
and
A. MIOTELLO
Dipartimento di Fisica, Unitgt GNSM-CISM, 1-38050 Povo, Trento, Italy
Received 30 May 1989; accepted for publication 20 June 1989
Coupled continuity equations for nitrogen atoms and vacancy fluxes are solved for known experimental conditions concerning the
depth profiles of nitrogen implanted in copper at different energies and temperatures. It is observed that for implantations carried
out at 200 ° C, nitrogen atoms possibly get trapped into vacancies during implantation and the vacancies tend to form clusters. The
surface peak observed in depth profile data is shown to be due to Gibbsian segregation. The nitrogen diffusion coefficient is observed
to be almost constant as temperature increases from -200 °C up to 200 o C.
1. Introduction
Ion implantation is a well established process
to introduce any element into any material, to a
depth which is controlled by the ion energy and
the stopping power of the substrate material.
However, the depth control is lost if thermally
activated radiation induced processes come into
play. In such a situation, the depth profiles of
implanted atoms can vary drastically from those
predicted by the LSS theory [1]. The LSS theory
takes into account the collisional effects which are
non-thermal and which take place within a time
period much less than a pico-second after the
primary collisions. On the contrary the radiation
induced effects are temperature dependent and
take place during a time period of a pico-second
to a milli-second after the primary collision. Radi-
ation induced redistribution of atoms can take
place due to preferential coupling between the
point defect flux and the flux of implanted atoms.
It is well known that during ion implantation,
numerous point defects (vacancies and intersti-
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(North-Holland)
tials) are produced. These defects migrate towards
sinks such as the surface, grain boundaries, etc.
The movement of the defects induces the trans-
port of implanted atoms. Experimentally solute
elements in irradiated alloys have been observed
to migrate towards [2] or away [3] from the sink.
There are various theories which relate the trans-
port of solute atoms to the flux of vacancies [4] or
interstitials [5]. However the lack of knowledge of
various parameters used in the theories, makes
quantitative prediction difficult. In such a case a
numerical solution of the transport equations to
fit experimental data can be used to obtain insight
into the process. In the present work the numeri-
cal approach is used for understanding the radia-
tion induced effects on the nitrogen implanted
copper system.
2. Theory
In order to describe nitrogen relocation in
copper during nitrogen implantation, both the bulk