Int. J. Curr. Res. Chem. Pharm. Sci. (2016). 3(3): 29-36
© 2016 IJCRCPS. All Rights Reserved 29
Research Article
ANTIOXIDANT, ANTIDIABETIC POTENTIAL AND QUANTIFICATION OF
LUPEOLL IN METHANOLIC EXTRACT OF ANETHUM SOWA LINN. (SEED)
I P TRIPATHI
1
, VANDANA PATHAK
1
, PUSHPENDRA KUMAR SHUKLA
2
AND
RUCHI DWIVEDI
1
1
Department of Physical Sciences, Mahatma Gandhi Chitrakoot Gramodaya Vishvavidyalaya, Satna,
Madhya Pradesh, India.
2
Pharmacognosy and Ethanopharmacology Division, CSIR-National Botanical Research Institute,
Lucknow-226001, India
*Corresponding Author: tripathi.ip@gmail.com
Abstract
Anethum sowa is widely used traditional medicine in many countries and in formulations of drugs. A simple, rapid, selective and
quantitative HPTLC method has been developed for determination of Lupeol in Anethum sowa and a scientific evaluation of its
traditional claims viz. anti oxidant and anti diabetic activity. The methanolic extract of Anethum sowa samples were applied on TLC
aluminium pre coated plate with Silica gel60 GF-254 and developed using Toluene:Ethyl acetate: Formic acid (5:3:0.8v/v) as a
mobile phase. Spectrophotometric evaluation was performed at 400 nm. Lupeol was resolved at Rf 0.58 ± 0.03 by pre
chromatographic derivatization with anisyldehyde sulphuric acid. Anti oxidant capacity, reducing power of the species increases
linearly with concentration, similar to standards. The IC50 value for the in vitro DPPH method was 1.22 ± 0.411 mg/ml. In vitro anti
diabetic activity was analyzed by starch-iodine assay and 3, 5-dinitrosalicylic acid method. In the starch-Iodine assay IC50 of
methanolic extract was found to be 252.9 ± 0.05 μg/ml and 0.236 ± 0.04 mg/ml for the DNS method.
Keywords: Anethum sowa, linolenic acid, DPPH; reducing power; total antioxidant capacity, α- amylase.
1. Introduction
Anethum sowa L. or dill, belonging to Apiaceae
(Umbelliferae) family, is an annual aromatic herb known
for culinary and medicinal use since ancient times. It is
an annual herb with pinnately divided leaves. The plant
grows up to a height of 150cm, stem is round and 2-5
branches arise from the base of stem and grow along
with the main stem. Flowers are yellow in colour. The
seeds, after ripening, attain light brown colour and emit
an aromatic odour. It is distributed in Germany,
Hungary, Netherlands, Pakistan and USA. In India, it is
found in Rajasthan, Gujarat, J&K, Orissa, Madhya
Pradesh and Punjab (Gupta et al., 2001). Dill seeds are
used, both whole and ground, as a condiment in soups,
salads, processed meats, sausages, spicy table sauces
and in dill picklings. Grounded seed is an ingredient of
seasoning. Dill stems and blossom heads are used for
dill pickling and for flavouring soups. The essential oil is
also used in the manufacture of soaps (Dahiya et al.,
2012). Medicinally, essential oil of dill is considered to be
carminative and specially used in control of flatulence,
colic and hiccups in infants and children. In recent years
the scientific literature reports pharmacological effects of
dill such as antibacterial (Singh et al., 2001),
antimycobacterial (Stavri et al., 2005), antioxidant (Lado
et al., 2004, Ghasemi et al., 2009)..
2. Materials and Methods
2.1 Chemicals and reagents
Ascorbic acid, Gallic acid, Euginol, Toluene. Ethyle
acetate, Formic acid, BHT (Butylated hydroxy toluene)
SOI: http://s-o-i.org/1.15/ijcrcps-2016-3-3-5